Technology Process of 4-[1H-imidazol-1-yl(4-phenyl-1H-pyrrol-3-yl)methyl]aniline
There total 4 articles about 4-[1H-imidazol-1-yl(4-phenyl-1H-pyrrol-3-yl)methyl]aniline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
at 45 ℃;
for 2h;
under 3040 Torr;
DOI:10.1021/jm00021a011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 28 percent / NaH / dimethylsulfoxide; diethyl ether / 0.5 h / Ambient temperature
2: 100 percent / LiAlH4 / tetrahydrofuran / 15 h / Ambient temperature
3: 65 percent / acetonitrile / 4 h / Ambient temperature
4: 100 percent / H2 / 10percent Pd/C / ethyl acetate / 2 h / 45 °C / 3040 Torr
With
lithium aluminium tetrahydride; hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide; ethyl acetate; acetonitrile;
DOI:10.1021/jm00021a011
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / LiAlH4 / tetrahydrofuran / 15 h / Ambient temperature
2: 65 percent / acetonitrile / 4 h / Ambient temperature
3: 100 percent / H2 / 10percent Pd/C / ethyl acetate / 2 h / 45 °C / 3040 Torr
With
lithium aluminium tetrahydride; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethyl acetate; acetonitrile;
DOI:10.1021/jm00021a011