1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)-

Base Information

Chemical Name:1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)-
CAS No.:60967-94-4
Molecular Formula:C18H17BrO4
Molecular Weight:377.2292
Hs Code.:
DSSTox Substance ID:DTXSID00209814
Wikidata:Q83084271

Synonyms:1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)-;60967-94-4;4-Bromo-1,2,3,4-tetrahydro-1,2-phenanthrenediol diacetate, (1alpha,2beta,4alpha)-;DTXSID00209814

Suppliers and Price of 1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)-

Chemical Property:

Vapor Pressure:5.22E-09mmHg at 25°C
Boiling Point:470.1°C at 760 mmHg
Flash Point:238.1°C
Density:1.46g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:376.03102
Heavy Atom Count:23
Complexity:466

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1CC(C2=C(C1OC(=O)C)C=CC3=CC=CC=C32)Br
Isomeric SMILES:CC(=O)O[C@H]1C[C@@H](C2=C([C@@H]1OC(=O)C)C=CC3=CC=CC=C32)Br

Technology Process of 1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)-

There total 2 articles about 1,2-Phenanthrenediol, 4-bromo-1,2,3,4-tetrahydro-, diacetate, (1alpha,2beta,4alpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60967-93-3,64069-85-8,64069-88-1
(+/-)-trans-1,2-diacetoxy-1,2,3,4-tetrahydro-phenanthrene

: 60967-94-4
4β-Brom-1β,2α-diacetoxy-1,2,3,4-tetrahydrophenanthren

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
DOI:10.1021/jo00424a036

Reference yield:

: 38399-10-9
3,4-dihydrophenanthrene

: 60967-94-4
4β-Brom-1β,2α-diacetoxy-1,2,3,4-tetrahydrophenanthren

Guidance literature:: Multi-step reaction with 2 steps

1: I₂

2: NBS, AIBN

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine;
DOI:10.1021/jo00424a036