(Z)-5-Tridecylidenefuran-2(5H)-one

Base Information

Chemical Name:(Z)-5-Tridecylidenefuran-2(5H)-one
CAS No.:77085-65-5
Molecular Formula:C₁₇H₂₈O₂
Molecular Weight:264.408
Hs Code.:
European Community (EC) Number:278-612-4
DSSTox Substance ID:DTXSID701283527
Nikkaji Number:J309.356E
Mol file:77085-65-5.mol

Synonyms:EINECS 278-612-4;77085-65-5;(Z)-5-Tridecylidenefuran-2(5H)-one;DTXSID701283527;(5Z)-5-Tridecylidenefuran-2(5H)-one;2(5H)-Furanone, 5-tridecylidene-, (Z)-

Suppliers and Price of (Z)-5-Tridecylidenefuran-2(5H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (Z)-5-Tridecylidenefuran-2(5H)-one

Chemical Property:

Vapor Pressure:2.54E-06mmHg at 25°C
Boiling Point:391°C at 760 mmHg
Flash Point:164.5°C
PSA：26.30000
Density:0.985g/cm³
LogP:5.29430
XLogP3:6.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:11
Exact Mass:264.208930132
Heavy Atom Count:19
Complexity:302

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCC=C1C=CC(=O)O1
Isomeric SMILES:CCCCCCCCCCCC/C=C\1/C=CC(=O)O1

Technology Process of (Z)-5-Tridecylidenefuran-2(5H)-one

There total 8 articles about (Z)-5-Tridecylidenefuran-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 77085-56-4
1-(5-methoxy-2-furyl)-n-tridecyl-1-ol

: 77085-62-2
cis-2-heptadecenoic acid-4-oxo-methyl ester

: 343224-46-4,77085-65-5
(Z)-2(5H)-furanone-5-(n-dodecylmethylene)

: 77085-61-1,77085-65-5
(E)-2(5H)-furanone-5-(n-dodecylmethylene)

Guidance literature:: With zinc(II) chloride; In water; acetone; at 20 ℃; for 0.25h; Yields of byproduct given;
DOI:10.1016/0040-4020(80)88034-3

Reference yield: 30.0%

: 77085-56-4
1-(5-methoxy-2-furyl)-n-tridecyl-1-ol

: 77085-62-2
cis-2-heptadecenoic acid-4-oxo-methyl ester

: 343224-46-4,77085-65-5
(Z)-2(5H)-furanone-5-(n-dodecylmethylene)

: 77085-61-1,77085-65-5
(E)-2(5H)-furanone-5-(n-dodecylmethylene)

Guidance literature:: With zinc(II) chloride; In water; acetone; at 20 ℃; for 0.25h; Yields of byproduct given;
DOI:10.1016/0040-4020(80)88034-3

Reference yield:

: 77085-53-1
1-(5-methoxy-2-furyl)-n-tridecyl-1-one

: 77085-61-1,77085-65-5
(E)-2(5H)-furanone-5-(n-dodecylmethylene)

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaBH₄ / methanol; dioxane; H₂O / 20 °C

2: ZnCl₂ / acetone; H₂O / 0.25 h / 20 °C

With sodium tetrahydroborate; zinc(II) chloride; In 1,4-dioxane; methanol; water; acetone;
DOI:10.1016/0040-4020(80)88034-3