4-(4-methylphenyl)dithiole-3-thione

Base Information

• Chemical Name: 4-(4-methylphenyl)dithiole-3-thione
• CAS No.: 3467-29-6
• Molecular Formula: C10H8 S3
• Molecular Weight: 224.372
• Hs Code.: 2930909090
• Mol file: 3467-29-6.mol

Synonyms:1,2-Dithiole-3-thione,4-p-tolyl- (6CI); 3H-1,2-Dithiole-3-thione, 4-p-tolyl- (7CI,8CI);4-p-Tolyl-1,2-dithiole-3-thione; 4-p-Tolyltrithione; NSC 40467

Chemical Property of 4-(4-methylphenyl)dithiole-3-thione

Chemical Property:

• Vapor Pressure: 1.66E-05mmHg at 25°C
• Melting Point: 122.5-123.0 °C
• Boiling Point: 375.7°Cat760mmHg
• Flash Point: 181°C
• PSA: 76.60000
• Density: 1.37g/cm³
• LogP: 4.37910

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(4-methylphenyl)dithiole-3-thione

There total 4 articles about 4-(4-methylphenyl)dithiole-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylisopropylbenzene (99-87-6) → 4-p-tolyl-1,2-dithiol-3-thione (3467-29-6)

Guidance literature:

With 1,3-Di(2-tolyl)guanidine; sulfur; at 185 ℃;

DOI:10.1021/ja01621a027

Reference yield:

1-methyl-4-isopropenylbenzene (1195-32-0) → 4-p-tolyl-1,2-dithiol-3-thione (3467-29-6)

Guidance literature:

With sulfur; at 260 ℃;

Reference yield:

4-methylisopropylbenzene (99-87-6) + 1,3-Di(2-tolyl)guanidine (97-39-2) → 4-p-tolyl-1,2-dithiol-3-thione (3467-29-6)

Guidance literature:

at 185 ℃;

DOI:10.1021/ja01621a027

upstream raw materials:

1-methyl-4-isopropenylbenzene

4-methylisopropylbenzene

1,3-Di(2-tolyl)guanidine

Downstream raw materials:

3-methylsulfanyl-4-p-tolyl-[1,2]dithiolylium

2-pyridin-2-yl-4-p-tolyl-2H-isothiazole-5-thione

2,4-di-p-tolyl-2H-isothiazole-5-thione

2-phenyl-4-p-tolyl-2H-isothiazole-5-thione