2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid

Base Information

Chemical Name:2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid
CAS No.:117125-43-6
Molecular Formula:C₁₇H₁₇NO₂S
Molecular Weight:299.393
Hs Code.:
DSSTox Substance ID:DTXSID00922298

Synonyms:BRN 4515329;117125-43-6;L-Alanine, N-((6,11-dihydrodibenzo(b,e)thiepin-11-yl)-;2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid;DTXSID00922298;N-(6,11-Dihydrodibenzo[b,E]thiepin-11-yl)alanine

Suppliers and Price of 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid

Chemical Property:

Vapor Pressure:5.86E-10mmHg at 25°C
Boiling Point:478.3°C at 760 mmHg
Flash Point:243.1°C
Density:1.3g/cm³
XLogP3:0.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:299.09799996
Heavy Atom Count:21
Complexity:376

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(=O)O)NC1C2=CC=CC=C2CSC3=CC=CC=C13
Isomeric SMILES:C[C@@H](C(=O)O)NC1C2=CC=CC=C2CSC3=CC=CC=C13

Technology Process of 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid

There total 2 articles about 2-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylamino)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 117125-40-3
ethyl 2-(6,11-dihydrodibenzothiepin-11-ylamino)propionate

: 117125-43-6
2-(6,11-dihydrodibenzothiepin-11-ylamino)propionic acid

Guidance literature:: With sodium hydroxide; water; acetic acid; In methanol; Heating;

Reference yield:

: 1745-53-5
11-amino-6,11-dihydrodibenzothiepin

: 117125-43-6
2-(6,11-dihydrodibenzothiepin-11-ylamino)propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Na₂CO₃ / toluene / 46 h / Heating

2: 91 percent / 1) 5M-NaOH, H₂O; 2) CH₃COOH / methanol / Heating

With sodium hydroxide; water; sodium carbonate; acetic acid; In methanol; toluene;