Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-cis-

Base Information

Chemical Name:Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-cis-
CAS No.:19245-69-3
Molecular Formula:C₁₁H₂₀O
Molecular Weight:168.279
Hs Code.:
Mol file:19245-69-3.mol

Synonyms:Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-, cis-; Cyclohexanol,5-tert-butyl-2-methylene-, cis- (8CI)

Suppliers and Price of Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-cis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-cis-

Chemical Property:

Vapor Pressure:0.029mmHg at 25°C
Boiling Point:217.1°Cat760mmHg
Flash Point:87.5°C
Density:0.9g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-cis-

There total 4 articles about Cyclohexanol,5-(1,1-dimethylethyl)-2-methylene-cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100052-57-1
2-Hydroxymethylen-5-tert-butyl-cyclohexanon-81)

: 19245-69-3,19245-70-6,60041-29-4,60041-30-7,71510-59-3,73803-32-4,73803-33-5
cis-2-hydroxy-4-tert-butylmethylenecyclohexane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1039/jr9610001650

Reference yield:

: 936-99-2
3-tert-butylcyclohexanone

: 19245-69-3,19245-70-6,60041-29-4,60041-30-7,71510-59-3,73803-32-4,73803-33-5
cis-2-hydroxy-4-tert-butylmethylenecyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / benzene

2: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; sodium methylate; In diethyl ether; benzene;
DOI:10.1039/jr9610001650

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 19245-69-3,19245-70-6,60041-29-4,60041-30-7,71510-59-3,73803-32-4,73803-33-5
cis-2-hydroxy-4-tert-butylmethylenecyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, 1 h, -78 deg C, 2.) 1 h, -78 deg C, 1 h, room temp.

2: 1.) KH, 2.) trimethyl phosphite, dimethylammonium chloride / 1.) THF, 1 h, 0 deg C, 2.) CH₃OH, 4 d, room temp.

With n-butyllithium; N,N-dimethylammonium chloride; potassium hydride; phosphorous acid trimethyl ester;