2-(furan-2-yl)-3,5-dimethylbenzyl methylcarbamate

Base Information

• Chemical Name: 2-(furan-2-yl)-3,5-dimethylbenzyl methylcarbamate
• CAS No.: 61518-02-3
• Molecular Formula: C₁₅H₁₇NO₃
• Molecular Weight: 259.305
• Mol file: 61518-02-3.mol

Synonyms:NSC315553

Chemical Property of 2-(furan-2-yl)-3,5-dimethylbenzyl methylcarbamate

Chemical Property:

• Vapor Pressure: 1.71E-06mmHg at 25°C
• Boiling Point: 396.4°Cat760mmHg
• Flash Point: 193.5°C
• Density: 1.119g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(furan-2-yl)-3,5-dimethylbenzyl methylcarbamate

There total 2 articles about 2-(furan-2-yl)-3,5-dimethylbenzyl methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethyl-2-(α-furyl)benzaldehyde (16191-40-5) → N-methylcarbamate of 3,5-dimethyl-2-(α-furyl)benzyl alcohol (61518-02-3)

Guidance literature:

Multi-step reaction with 2 steps

1: KBH₄ / methanol / Heating

2: trimethylamine / diethyl ether

With potassium borohydride; trimethylamine; In methanol; diethyl ether;

DOI:10.1002/mrc.1270180104

Reference yield:

3,5-dimethyl-2-(α-furyl)benzyl alcohol (16191-45-0) + methyl isocyanate (624-83-9) → N-methylcarbamate of 3,5-dimethyl-2-(α-furyl)benzyl alcohol (61518-02-3)

Guidance literature:

trimethylamine; In diethyl ether;

DOI:10.1002/mrc.1270180104

upstream raw materials:

3,5-dimethyl-2-(α-furyl)benzyl alcohol

methyl isocyanate

3,5-dimethyl-2-(α-furyl)benzaldehyde