Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl-

Base Information

Chemical Name:Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl-
CAS No.:97906-59-7
Molecular Formula:C₁₂H₁₃NO₃
Molecular Weight:219.24
Hs Code.:
DSSTox Substance ID:DTXSID80243337
Mol file:97906-59-7.mol

Synonyms:Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl-;2-Amino-2-(3-hydroxybenzyl)penta-3,4-dienoic acid;97906-59-7;3-Hydroxy-alpha-1,2-propadienylphenylalanine;DTXSID80243337;LS-105746

Suppliers and Price of Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl-

Chemical Property:

Vapor Pressure:6.18E-09mmHg at 25°C
Boiling Point:451.4°C at 760 mmHg
Flash Point:226.8°C
PSA：83.55000
Density:1.226g/cm³
LogP:1.75820
XLogP3:-1.5
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:219.08954328
Heavy Atom Count:16
Complexity:309

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C=CC(CC1=CC(=CC=C1)O)(C(=O)O)N
Isomeric SMILES:C=C=C[C@](CC1=CC(=CC=C1)O)(C(=O)O)N

Technology Process of Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl-

There total 6 articles about Phenylalanine, 3-hydroxy-alpha-1,2-propadienyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzoic acid 3-(2-amino-2-methoxycarbonyl-penta-3,4-dienyl)-phenyl ester

: 97906-59-7
α-allenic m-tyrosine

Guidance literature:: With sodium hydroxide; In methanol;
DOI:10.1021/ja00321a062

Reference yield:

: 775-06-4,29562-33-2
D/L-3-hydroxy-phenylalanine

: 97906-59-7
α-allenic m-tyrosine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) OH^(1-); 2.) DCC, DMPA

2: Ph₃P, CCl₄, NEt₃ / acetonitrile / Ambient temperature

3: NEt₃

4: Et₃O⁽¹⁺⁾*BF₄^(1-), 10percent HOAc / CH₂Cl₂

5: 1.0 N NaOH / methanol

With tetrachloromethane; sodium hydroxide; 0,2,4-dichlorophenyl-0-methylisopropylamidothiophosphate; hydroxide; triethyloxonium fluoroborate; acetic acid; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00321a062

Reference yield:

: Benzoic acid 3-(5-oxo-2-phenyl-4-propa-1,2-dienyl-4,5-dihydro-oxazol-4-ylmethyl)-phenyl ester

: 97906-59-7
α-allenic m-tyrosine

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃

2: Et₃O⁽¹⁺⁾*BF₄^(1-), 10percent HOAc / CH₂Cl₂

3: 1.0 N NaOH / methanol

With sodium hydroxide; triethyloxonium fluoroborate; acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja00321a062