3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline

Base Information

Chemical Name:3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline
CAS No.:77831-91-5
Molecular Formula:C₁₅H₂₁NO
Molecular Weight:231.338
Hs Code.:
Mol file:77831-91-5.mol

Synonyms:3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline

Suppliers and Price of 3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline

Chemical Property:

Vapor Pressure:1.74E-05mmHg at 25°C
Boiling Point:353.6°C at 760 mmHg
Flash Point:166.3°C
Density:1.088g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline

There total 5 articles about 3,10b-dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzo(f)isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77831-87-9
2-<2-(4'-Methoxyphenyl)-ethyl>-acrylsaeureethylester

: 72311-28-5,77831-91-5
cis-3,10b-Dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzoisochinolin

Guidance literature:: Multi-step reaction with 5 steps

1: 58.9 percent / ethanol / 20 h / 105 °C / 30400 Torr

2: 70.7 percent / 12 h / 110 °C

3: 83.6 percent / NaH, NaOH

5: 48percent aq. HBr / 60 h / Heating

With sodium hydroxide; hydrogen bromide; sodium hydride; In ethanol;
DOI:10.1002/ardp.19813140303

Reference yield:

: 1,4-Dimethyl-3-<2-(4'-methoxyphenyl)ethyl>-4-hydroxypiperidine

: 72311-28-5,77831-91-5
cis-3,10b-Dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzoisochinolin

Guidance literature:: With hydrogen bromide; for 60h; Yield given; Heating;
DOI:10.1002/ardp.19813140303

Reference yield:

: 77831-90-4
1-Methyl-3-<2-(4'-methoxyphenyl)-ethyl>-4-piperidon

: 72311-28-5,77831-91-5
cis-3,10b-Dimethyl-9-hydroxy-1,2,3,4,4a,5,6,10b-octahydrobenzoisochinolin

Guidance literature:: Multi-step reaction with 2 steps

2: 48percent aq. HBr / 60 h / Heating

With hydrogen bromide;
DOI:10.1002/ardp.19813140303