1-(4-chlorophenyl)-6-methyl-4-oxo-pyridazine-3-carboxylate

Base Information

Chemical Name:1-(4-chlorophenyl)-6-methyl-4-oxo-pyridazine-3-carboxylate
CAS No.:68254-10-4
Molecular Formula:C12H8ClN2O3-
Molecular Weight:264.668
Hs Code.:2933990090
Mol file:68254-10-4.mol

Synonyms:UNII-Q6E8BE2U25;1-(4-chlorophenyl)-6-methyl-4-oxopyridazine-3-carboxylic acid;1-(4-chlorophenyl)-6-methyl-4-oxo-1,4-dihydropyridazine-3-carboxylic acid;1-(4-chlorophenyl)-1,4-dihydro-6-methyl-4-oxopyridazine-3-carboxylic acid;1-(4-chlorophenyl)-1,4-dihydro-6-methyl-4-oxo-3-pyridazinecarboxylic acid;Fenridazon;

Suppliers and Price of 1-(4-chlorophenyl)-6-methyl-4-oxo-pyridazine-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(4-CHLOROPHENYL)-6-METHYL-4-OXO-1,4-DIHYDROPYRIDAZINE-3-CARBOXYLIC ACID 95.00%
2.5G
$ 983.88

American Custom Chemicals Corporation
1-(4-CHLOROPHENYL)-6-METHYL-4-OXO-1,4-DIHYDROPYRIDAZINE-3-CARBOXYLIC ACID 95.00%
1G
$ 290.85

AK Scientific
Fenridazon
250mg
$ 203.00

AK Scientific
Fenridazon
100mg
$ 172.00

Total 8 raw suppliers

Chemical Property of 1-(4-chlorophenyl)-6-methyl-4-oxo-pyridazine-3-carboxylate

Chemical Property:

Vapor Pressure:5.21E-09mmHg at 25°C
Melting Point:234.3-235.1℃ (ethanol )
Boiling Point:453.4°C at 760 mmHg
PKA:0.17±0.20(Predicted)
Flash Point:228°C
PSA：72.19000
Density:1.43±0.1 g/cm3(Predicted)
LogP:1.89250

Purity/Quality:

97% ^*data from raw suppliers

1-(4-CHLOROPHENYL)-6-METHYL-4-OXO-1,4-DIHYDROPYRIDAZINE-3-CARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4-chlorophenyl)-6-methyl-4-oxo-pyridazine-3-carboxylate

There total 6 articles about 1-(4-chlorophenyl)-6-methyl-4-oxo-pyridazine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 675-10-5
4-hydroxy-6-methyl-2-pyron

: 106-47-8
4-chloro-aniline

: 68254-10-4
1-(4-chlorophenyl)-1,4-dihydro-4-oxo-6-methylpyridazine-3-carboxylic acid

Guidance literature:: With sodium carbonate; aniline; sodium nitrite; In hydrogenchloride; water;

Reference yield:

: 78242-72-5
C₁₂H₉ClN₂O₃

: 68254-10-4
1-(4-chlorophenyl)-1,4-dihydro-4-oxo-6-methylpyridazine-3-carboxylic acid

Guidance literature:: In water; at 110 ℃; for 3h;
DOI:10.1002/ardp.200900290

Reference yield:

: 771-03-9
3-acetyl-4-hydroxy-6-methyl-2H-pyran-2-one

: 68254-10-4
1-(4-chlorophenyl)-1,4-dihydro-4-oxo-6-methylpyridazine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / water / 0.22 h / 130 °C / Flow reactor

2.1: sodium nitrite; hydrogenchloride / water / 0.07 h / 10 °C / Flow reactor

2.2: 25 °C / Flow reactor

3.1: potassium carbonate / water / 85 °C / Flow reactor

With hydrogenchloride; sulfuric acid; potassium carbonate; sodium nitrite; In water;
DOI:10.1002/ejoc.201600222