(4R)-4α-[(R)-3-Hydroxybutyl]-5β-hydroxymethyl-3,3-dimethylcyclohexanone

Base Information

Chemical Name:(4R)-4α-[(R)-3-Hydroxybutyl]-5β-hydroxymethyl-3,3-dimethylcyclohexanone
CAS No.:70142-91-5
Molecular Formula:C13H24O3
Molecular Weight:228.33
Hs Code.:
Mol file:70142-91-5.mol

Synonyms:Nigakialkohol;Nigaki-Alkohol;(4R,5S)-4-((R)-3-Hydroxy-butyl)-5-hydroxymethyl-3,3-dimethyl-cyclohexanone;

Suppliers and Price of (4R)-4α-[(R)-3-Hydroxybutyl]-5β-hydroxymethyl-3,3-dimethylcyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (4R)-4α-[(R)-3-Hydroxybutyl]-5β-hydroxymethyl-3,3-dimethylcyclohexanone

Chemical Property:

PSA：57.53000
LogP:1.76120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4R)-4α-[(R)-3-Hydroxybutyl]-5β-hydroxymethyl-3,3-dimethylcyclohexanone

There total 2 articles about (4R)-4α-[(R)-3-Hydroxybutyl]-5β-hydroxymethyl-3,3-dimethylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 128533-22-2
(1S,4R,5S)-4-((R)-3-Hydroxy-butyl)-5-hydroxymethyl-3,3-dimethyl-cyclohexanol

: 70142-91-5
Nigakialcohol

Guidance literature:: With Molsin (protease type XIII from Aspergillus saitoi); In ethanol; at 37 ℃; for 96h;
DOI:10.1248/cpb.38.830

Reference yield:

: Melia-ioniside A

: 70142-91-5
Nigakialcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 10percent H₂SO₄ / methanol

2: 84 percent / Molsin (protease type XIII from Aspergillus saitoi) / ethanol / 96 h / 37 °C

With Molsin (protease type XIII from Aspergillus saitoi); sulfuric acid; In methanol; ethanol;
DOI:10.1248/cpb.38.830