4'-Methyl-4-dimethylaminostilbene

Base Information

• Chemical Name: 4'-Methyl-4-dimethylaminostilbene
• CAS No.: 7378-54-3
• Molecular Formula: C₁₇H₁₉N
• Molecular Weight: 237.345
• DSSTox Substance ID: DTXSID60994719
• Mol file: 7378-54-3.mol

Synonyms:N,N,4'-Trimethyl-4-stilbenamine;7378-54-3;N,N-dimethyl-4-[2-(4-methylphenyl)ethenyl]aniline;BRN 2724433;4'-Methyl-4-dimethylaminostilbene;4-Stilbenamine, N,N,4'-trimethyl-;SCHEMBL10770661;DTXSID60994719

Chemical Property of 4'-Methyl-4-dimethylaminostilbene

Chemical Property:

• Vapor Pressure: 5.99E-06mmHg at 25°C
• Refractive Index: 1.4870 (estimate)
• Boiling Point: 379.1°C at 760 mmHg
• Flash Point: 153.7°C
• PSA: 3.24000
• Density: 1.045g/cm³
• LogP: 4.23140
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 237.151749610
• Heavy Atom Count: 18
• Complexity: 253

Purity/Quality:

99% ^*data from raw suppliers

N,N,4'-TRIMETHYL-4-STILBENAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)C=CC2=CC=C(C=C2)N(C)C

Technology Process of 4'-Methyl-4-dimethylaminostilbene

There total 1 articles about 4'-Methyl-4-dimethylaminostilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl 4-N,N-dimethylaminobenzylphosphonate (32264-24-7) + 4-methyl-benzaldehyde (104-87-0) → 4-N,N-dimethylamino-4'-methylstilbene (7378-54-3)

Guidance literature:

With sodium ethanolate; In N,N-dimethyl-formamide;

DOI:10.1002/poc.1660

Reference yield: 21.0%

4-N,N-dimethylamino-4'-methylstilbene (7378-54-3) → 4,4'-((2S,3R,4R,5S)-3,4-di-p-tolyltetrahydrofuran-2,5-diyl)bis(N,N-dimethylaniline) + 4,4'-((2R,3S,4R,5S)-3,4-di-p-tolyltetrahydrofuran-2,5-diyl)bis(N,N-dimethylaniline) (1608492-57-4) + (2S,3S)-4,4-bis(4-(dimethylamino)phenyl)-2,3-di-p-tolylbutanal + 4,4'-((2R,3R,4R,5S)-3,4-di-p-tolyltetrahydrofuran-2,5-diyl)bis(N,N-dimethylaniline)

Guidance literature:

With lithium perchlorate; In acetonitrile; Overall yield = 58 %; Electrolysis; Inert atmosphere;

DOI:10.1021/jo500559r

upstream raw materials:

diethyl 4-N,N-dimethylaminobenzylphosphonate

4-methyl-benzaldehyde

Downstream raw materials:

4,4'-((2R,3S,4R,5S)-3,4-di-p-tolyltetrahydrofuran-2,5-diyl)bis(N,N-dimethylaniline)

Refernces