(E)-1-(3,4,5-trimethoxyphenyl)-N-[(Z)-(3,4,5-trimethoxyphenyl)methylideneamino]methanimine

Base Information

• Chemical Name: (E)-1-(3,4,5-trimethoxyphenyl)-N-[(Z)-(3,4,5-trimethoxyphenyl)methylideneamino]methanimine
• CAS No.: 7251-01-6
• Molecular Formula: C20H24N2O6
• Molecular Weight: 388.42
• NSC Number: 30431
• DSSTox Substance ID: DTXSID40422348
• Wikidata: Q82234245

Synonyms:NSC30431;7251-01-6;DTXSID40422348;NSC-30431

Chemical Property of (E)-1-(3,4,5-trimethoxyphenyl)-N-[(Z)-(3,4,5-trimethoxyphenyl)methylideneamino]methanimine

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 502.443°C at 760 mmHg
• Flash Point: 206.182°C
• Density: 1.141g/cm³
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 9
• Exact Mass: 388.16343649
• Heavy Atom Count: 28
• Complexity: 431

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC(=CC(=C1OC)OC)C=NN=CC2=CC(=C(C(=C2)OC)OC)OC
• Isomeric SMILES: COC1=CC(=CC(=C1OC)OC)/C=N/N=C\C2=CC(=C(C(=C2)OC)OC)OC

Technology Process of (E)-1-(3,4,5-trimethoxyphenyl)-N-[(Z)-(3,4,5-trimethoxyphenyl)methylideneamino]methanimine

There total 8 articles about (E)-1-(3,4,5-trimethoxyphenyl)-N-[(Z)-(3,4,5-trimethoxyphenyl)methylideneamino]methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3,4,5-trimethoxy-benzaldehyde (86-81-7) → 3,4,5-trimethoxybenzaldehyde N-[-(3,4,5-trimethoxyphenyl)methylidene]hydrazone (7251-01-6)

Guidance literature:

With bismuth(III) chloride; hydrazine; In water; at 20 ℃; for 0.0166667h; Sonication; Green chemistry;

DOI:10.1016/j.ultsonch.2013.12.011

Reference yield: 97.0%

3,4,5-trimethoxy-benzaldehyde (86-81-7) → (1E, 2E)-1,2-bis(3,4,5-trimethoxybenzylidene)hydrazine (7251-01-6)

Guidance literature:

With hydrazine hydrate; triethylamine sulfate; In neat (no solvent); at 120 ℃; for 0.5h;

DOI:10.1039/c4nj01666a

Reference yield: 90.0%

(E)-2-(3,4,5-trimethoxybenzylidene)hydrazine carboxamide (81824-93-3) → (1E, 2E)-1,2-bis(3,4,5-trimethoxybenzylidene)hydrazine (7251-01-6)

Guidance literature:

at 160 - 180 ℃; Autoclave; Green chemistry;

DOI:10.1080/00397911.2015.1113297

upstream raw materials:

3,4,5-trimethoxy-benzaldehyde

(E)-2-(3,4,5-trimethoxybenzylidene)hydrazine carboxamide

(3,4,5-trimethoxyphenyl)methanol

3,4,5-trimethoxybenzonitrile

Downstream raw materials:

2,5-bis(3,4,5-trimethoxyphenyl)-1,3,4-thiadiazole

3,3',4,4',5,5'-hexamethoxystilbene

7,11-bis-(3,4,5-trimethoxyphenyl)-3,3-dimethyl-2,4-dioxaspiro[5.5]undecane-1,5,9-trione

Eudesmic acid

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