ETHYL 4-CHLORO-3-TRIFLUOROMETHYLCARBANILATE

Base Information

• Chemical Name: ETHYL 4-CHLORO-3-TRIFLUOROMETHYLCARBANILATE
• CAS No.: 18585-06-3
• Molecular Formula: C10H9 Cl F3 N O2
• Molecular Weight: 267.63
• Hs Code.: 2924299090
• Mol file: 18585-06-3.mol

Synonyms:Carbamicacid, [4-chloro-3-(trifluoromethyl)phenyl]-, ethyl ester (9CI); Carbanilic acid,4-chloro-3-(trifluoromethyl)-, ethyl ester (8CI)

Chemical Property of ETHYL 4-CHLORO-3-TRIFLUOROMETHYLCARBANILATE

Chemical Property:

• Vapor Pressure: 0.0193mmHg at 25°C
• Boiling Point: 252.5°C at 760 mmHg
• PKA: 12.44±0.70(Predicted)
• Flash Point: 106.5°C
• PSA: 38.33000
• Density: 1.402g/cm³
• LogP: 4.00020

Purity/Quality:

≥99% ^*data from raw suppliers

Ethyl(4-Chloro-3-(trifluoromethyl)phenyl)carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 4-CHLORO-3-TRIFLUOROMETHYLCARBANILATE

There total 1 articles about ETHYL 4-CHLORO-3-TRIFLUOROMETHYLCARBANILATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-2-(trifluoromethyl)benzene (88-16-4) + urethane (51-79-6) → ethyl (4-chloro-3-(trifluoromethyl)phenyl)carbamate (18585-06-3) + C10H9ClF3NO2

Guidance literature:

With tert.-butylnitrite; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 25 ℃; for 24h; Overall yield = 26 %; Irradiation;

DOI:10.1002/chem.201705442

Reference yield:

ethyl (4-chloro-3-(trifluoromethyl)phenyl)carbamate (18585-06-3) → 1-(4-chloro-3-(trifluoromethyl)phenyl)-3-hydroxyurea (1129683-96-0)

Guidance literature:

With hydroxylamine hydrochloride; acetic acid; for 12h; Heating / reflux;

upstream raw materials:

1-chloro-2-(trifluoromethyl)benzene

urethane

Downstream raw materials:

1-(4-chloro-3-(trifluoromethyl)phenyl)-3-hydroxyurea

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