2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane

Base Information

Chemical Name:2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane
CAS No.:5694-99-5
Molecular Formula:C10H20O3
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID40972393
Nikkaji Number:J42.155C
Mol file:5694-99-5.mol

Synonyms:5694-99-5;2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane;2-(2-methyl-1,3-dioxolan-2-yl)hexan-1-ol;1,3-Dioxolane, 2-methyl-2-(1'-methylolpentyl)-;DTXSID40972393

Suppliers and Price of 2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-METHYL-2-(1'-METHYLOLPENTYL)-1,3-DIOXOLANE 95.00%
5MG
$ 498.84

Total 3 raw suppliers

Chemical Property of 2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane

Chemical Property:

Vapor Pressure:0.00184mmHg at 25°C
Boiling Point:259.9°C at 760 mmHg
Flash Point:125.7°C
PSA：38.69000
Density:0.999g/cm³
LogP:1.54810
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:188.14124450
Heavy Atom Count:13
Complexity:141

Purity/Quality:: 2-METHYL-2-(1'-METHYLOLPENTYL)-1,3-DIOXOLANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC(CO)C1(OCCO1)C

Technology Process of 2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane

There total 3 articles about 2-Methyl-2-(1'-methylolpentyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₂₀O₄

: 5694-99-5
2-(2-methyl-1,3-dioxolan-2-yl)hexan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/acs.orglett.6b00151

Reference yield:

: 5694-99-5
2-(2-methyl-1,3-dioxolan-2-yl)hexan-1-ol

Guidance literature:: With ethanol; sodium;
DOI:10.1002/hlca.19490320641 DOI:10.1021/ja01178a009

Reference yield:

: 32798-42-8
methyl α-butylacetoacetate

: 5694-99-5
2-(2-methyl-1,3-dioxolan-2-yl)hexan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 18 h / Reflux; Dean-Stark

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1021/acs.orglett.6b00151