1-Pentofuranosyl-1h-benzotriazole

Base Information

Chemical Name:1-Pentofuranosyl-1h-benzotriazole
CAS No.:22596-06-1
Molecular Formula:C11H13 N3 O4
Molecular Weight:251.2386
Hs Code.:
NSC Number:122817
DSSTox Substance ID:DTXSID20298386
Mol file:22596-06-1.mol

Synonyms:1-pentofuranosyl-1h-benzotriazole;2-(benzotriazol-1-yl)-5-(hydroxymethyl)oxolane-3,4-diol;22596-06-1;NSC122817;DTXSID20298386;STL435983;AKOS037480940;NSC-122817;1H-Benzotriazole, 1-.beta.-D-ribofuranosyl-;2-(1H-1,2,3-BENZOTRIAZOL-1-YL)-5-(HYDROXYMETHYL)TETRAHYDRO-3,4-FURANDIOL

Suppliers and Price of 1-Pentofuranosyl-1h-benzotriazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-Pentofuranosyl-1h-benzotriazole

Chemical Property:

Vapor Pressure:5.15E-14mmHg at 25°C
Boiling Point:574°C at 760 mmHg
Flash Point:300.9°C
Density:1.75g/cm³
XLogP3:-0.5
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:251.09060590
Heavy Atom Count:18
Complexity:306

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)N=NN2C3C(C(C(O3)CO)O)O

Technology Process of 1-Pentofuranosyl-1h-benzotriazole

There total 12 articles about 1-Pentofuranosyl-1h-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 123499-58-1
1H-benzotriazole mononucleotide ammonium salt

: 22596-06-1
1-β-Ribofuranosyl-benzotriazol

Guidance literature:: With 5'-nucleotidase; tris hydrochloride; magnesium chloride; In water; at 37 ℃; for 8h; pH: 9.2;

Reference yield: 85.3%

: 54548-46-8
(2R,3R,4R,5R)-4-(acetyloxty)-2-[(acetyloxy)methyl]-5-(1H-1,2,3-benzotriazol-1-yl)tetrahydro-3-furanyl acetate

: 22596-06-1
1-β-Ribofuranosyl-benzotriazol

Guidance literature:: With ammonia; In methanol; at 20 ℃;

Reference yield:

: methyl 2,3,5-tris-O-(p-chlorobenzoyl)-D-ribofuranoside

: 22596-06-1
1-β-Ribofuranosyl-benzotriazol

Guidance literature:: Multi-step reaction with 3 steps

1: 81.3 percent / conc. H₂SO₄ / acetic acid / 2 h / Ambient temperature

2: 44.5 percent / p-toluenesulfonic acid / 0.17 h / 160 °C / 20 Torr

3: NaOMe, MeOH / Ambient temperature

With methanol; sulfuric acid; sodium methylate; toluene-4-sulfonic acid; In acetic acid;
DOI:10.1021/jm00102a006