2-(5-Acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate

Base Information

Chemical Name:2-(5-Acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate
CAS No.:92582-15-5
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:
NSC Number:115701
DSSTox Substance ID:DTXSID50297362

Synonyms:92582-15-5;2-(5-acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate;NSC115701;DTXSID50297362;NSC-115701

Suppliers and Price of 2-(5-Acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(5-Acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate

Chemical Property:

Vapor Pressure:3.57E-06mmHg at 25°C
Boiling Point:386.3°C at 760 mmHg
Flash Point:170.3°C
Density:1.153g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:262.12050905
Heavy Atom Count:19
Complexity:374

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=CC2=C(C=C1)OC(C2)C(C)(C)OC(=O)C

Technology Process of 2-(5-Acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate

There total 8 articles about 2-(5-Acetyl-2,3-dihydro-1-benzofuran-2-yl)propan-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 24007-50-9
2-(1-hydroxy-1-methylethyl)-2,3-dihydrobenzofuran

: 108-24-7
acetic anhydride

: 92582-15-5
1-(5-acetyl-2,3-dihydro-2-benzofuranyl)-1-methylethyl acetate

Guidance literature:: With tin(IV) chloride; In benzene; at 0 ℃; for 0.5h;
DOI:10.1246/bcsj.58.3282

Reference yield:

: 19863-70-8,104518-93-6
(RS)-2-acetyl-2,3-dihydrobenzofuran

: 92582-15-5
1-(5-acetyl-2,3-dihydro-2-benzofuranyl)-1-methylethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / diethyl ether / 1 h / Ambient temperature

2: 82 percent / SnCl₄ / benzene / 0.5 h / 0 °C

With tin(IV) chloride; In diethyl ether; benzene;
DOI:10.1246/bcsj.58.3282

Reference yield:

: 16198-39-3
(+/-)-2-ethenyl-2,3-dihydrobenzofuran

: 92582-15-5
1-(5-acetyl-2,3-dihydro-2-benzofuranyl)-1-methylethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / Pd(OCOCF₃)(OOBu^t), Bu^tOOH / benzene / 16 h / 50 °C

2: 70 percent / diethyl ether / 1 h / Ambient temperature

3: 82 percent / SnCl₄ / benzene / 0.5 h / 0 °C

With tert.-butylhydroperoxide; Pd(OCOCF₃)(OOBu^t); tin(IV) chloride; In diethyl ether; benzene;
DOI:10.1246/bcsj.58.3282