Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine

Base Information

Chemical Name:Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine
CAS No.:122033-01-6
Molecular Formula:C₁₄H₁₀N₄S
Molecular Weight:266.326
Hs Code.:
DSSTox Substance ID:DTXSID80153482
Wikidata:Q83020365
Mol file:122033-01-6.mol

Synonyms:122033-01-6;Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine;BRN 5571453;8-Amino-(1,2,4)-triazolo(4,3-d)(b,e)-1,4-dibenzothiazepine;13-thia-2,4,5-triazatetracyclo[12.4.0.02,6.07,12]octadeca-1(14),3,5,7,9,11,15,17-octaen-17-amine;DTXSID80153482;CODICMXJADBLMH-UHFFFAOYSA-N;LS-61514;Dibenzo[b,f][1,2,4]triazolo[4,3-d][1,4]thiazepin-6-amine

Suppliers and Price of Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DIBENZO(B,F)-1,2,4-TRIAZOLO(4,3-D)(1,4)THIAZEPIN-6-AMINE 95.00%
5MG
$ 499.00

Total 1 raw suppliers

Chemical Property of Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine

Chemical Property:

Vapor Pressure:7.3E-14mmHg at 25°C
Boiling Point:589.3°C at 760 mmHg
Flash Point:310.2°C
PSA：82.03000
Density:1.51g/cm³
LogP:3.56230
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:266.06261751
Heavy Atom Count:19
Complexity:339

Purity/Quality:: DIBENZO(B,F)-1,2,4-TRIAZOLO(4,3-D)(1,4)THIAZEPIN-6-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=NN=CN3C4=C(S2)C=CC(=C4)N

Technology Process of Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine

There total 3 articles about Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepin-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122032-99-9
8-amino-11-chloro-10,11-dihydro-dibenzo<1,4>thiazepine

: 122033-01-6
8-amino-(1,2,4)-triazolo<4,3-d>-1,4-dibenzothiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / NH₂NH₂*H₂O / glycerol / 6 h / Heating

2: 60 percent / dioxane / 4 h / Heating

With hydrazine hydrate; In 1,4-dioxane; glycerol;

Reference yield:

: 105554-89-0
8-amino-10,11-dihydro-dibenzo<1,4>thiazepin-11-one

: 122033-01-6
8-amino-(1,2,4)-triazolo<4,3-d>-1,4-dibenzothiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / HCl gas / POCl₃ / 1.5 h / Heating

2: 68 percent / NH₂NH₂*H₂O / glycerol / 6 h / Heating

3: 60 percent / dioxane / 4 h / Heating

With hydrogenchloride; hydrazine hydrate; In 1,4-dioxane; glycerol; trichlorophosphate;

Reference yield:

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 122033-01-6
8-amino-(1,2,4)-triazolo<4,3-d>-1,4-dibenzothiazepine

Guidance literature:: Multi-step reaction with 4 steps

2: 70 percent / HCl gas / POCl₃ / 1.5 h / Heating

3: 68 percent / NH₂NH₂*H₂O / glycerol / 6 h / Heating

4: 60 percent / dioxane / 4 h / Heating

With hydrogenchloride; hydrazine hydrate; In 1,4-dioxane; glycerol; trichlorophosphate;