4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate

Base Information

Chemical Name:4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate
CAS No.:104761-48-0
Molecular Formula:C10H10BBrF4N2
Molecular Weight:324.9084
Hs Code.:
DSSTox Substance ID:DTXSID10146701

Synonyms:4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate;104761-48-0;1-Naphthalenediazonium, 4-bromo-5,6,7,8-tetrahydro-, tetrafluoroborate(1-);DTXSID10146701;C10-H10-B-Br-F4-N2

Suppliers and Price of 4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:0
Exact Mass:324.00565
Heavy Atom Count:18
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[B-](F)(F)(F)F.C1CCC2=C(C=CC(=C2C1)[N+]#N)Br

Technology Process of 4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate

There total 1 articles about 4-Bromo-5,6,7,8-tetrahydronaphthalene-1-diazonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 104761-46-8
4-Bromo-5,6,7,8-tetrahydro-naphthalen-1-ylamine; hydrochloride

: 104761-48-0
C₁₀H₁₀BrN₂⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: With hydrogenchloride; tetrafluoroboric acid; sodium nitrite; In water; at 0 ℃; for 0.25h;
DOI:10.1021/jo00374a001

Reference yield: 82.0%

: 104761-48-0
C₁₀H₁₀BrN₂⁽¹⁺⁾*BF₄^(1-)

: 104761-49-1
1-bromo-4-fluoro-5,6,7,8-tetrahydronaphthalene

Guidance literature:: at 170 ℃; for 0.333333h;
DOI:10.1021/jo00374a001

Reference yield:

: 104761-48-0
C₁₀H₁₀BrN₂⁽¹⁺⁾*BF₄^(1-)

: 104761-50-4
2-<(4-fluoro-5,6,7,8-tetrahydro-1-naphthalenyl)carbonyl>benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 0.33 h / 170 °C

2: 1.) ethylene dibromide, Mg / 1.) THF, benzene, reflux, 45 min, 2.) THF, benzene, reflux, 5 h

With magnesium; ethylene dibromide;
DOI:10.1021/jo00374a001