2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl-

Base Information

Chemical Name:2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl-
CAS No.:87373-48-6
Molecular Formula:C12H14N2
Molecular Weight:186.253
Hs Code.:
DSSTox Substance ID:DTXSID201007516
Nikkaji Number:J744.567I
Wikidata:Q83003572

Synonyms:87373-48-6;2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl-;2,3-Diazabicyclo[2.2.2]oct-2-ene, 1-phenyl-;1-phenyl-2,3-diazabicyclo[2.2.2]oct-2-ene;DTXSID201007516

Suppliers and Price of 2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl-

Chemical Property:

Vapor Pressure:0.00697mmHg at 25°C
Boiling Point:279°C at 760 mmHg
Flash Point:114.4°C
Density:1.2g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:186.115698455
Heavy Atom Count:14
Complexity:233

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2(CCC1N=N2)C3=CC=CC=C3

Technology Process of 2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl-

There total 3 articles about 2,3-Diazabicyclo(2.2.2)oct-2-ene, 1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15619-32-6
1-phenyl-cyclohexa-1,3-diene

: 87373-48-6
1-phenyl-2,3-diazabicyclo<2.2.2>oct-2-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 44.1 percent / ethyl acetate / 25 °C

2: 100 percent / H₂ / Pd/C / tetrahydrofuran / 25 °C / 760 Torr

3: 1.) KOH, 2.) CuCl₂, 3.) NH₄OH

With potassium hydroxide; ammonium hydroxide; hydrogen; copper dichloride; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/ja00362a014

Reference yield:

: 87433-37-2
1-phenyl-4-methyl-2,4,6-triaza<5.2.2.0^2,6>tricycloundec-8-ene-3,5-dione

: 87373-48-6
1-phenyl-2,3-diazabicyclo<2.2.2>oct-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / tetrahydrofuran / 25 °C / 760 Torr

2: 1.) KOH, 2.) CuCl₂, 3.) NH₄OH

With potassium hydroxide; ammonium hydroxide; hydrogen; copper dichloride; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/ja00362a014

Reference yield:

: 87433-38-3
1-phenyl-4-methyl-2,4,6-triaza<5.2.2.0^2,6>tricycloundecane-3,5-dione

: 87373-48-6
1-phenyl-2,3-diazabicyclo<2.2.2>oct-2-ene

Guidance literature:: With potassium hydroxide; ammonium hydroxide; copper dichloride; Yield given. Multistep reaction;
DOI:10.1021/ja00362a014