methyl 2-[(Z)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbodithioate

Base Information

Chemical Name:methyl 2-[(Z)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbodithioate
CAS No.:26151-73-5
Molecular Formula:C9H10 N2 O S2
Molecular Weight:226.323
Hs Code.:

Synonyms:Carbazicacid, 3-salicylidenedithio-, methyl ester (8CI); Hydrazinecarbodithioic acid,[(2-hydroxyphenyl)methylene]-, methyl ester (9CI); Methyl3-(o-hydroxybenzylidene)dithiocarbazate; Methyl salicylidenedithiocarbazate;NSC 147440; S-Methyl 3-(2-hydroxybenzylidene)dithiocarbazate; S-Methyl3-(2-hydroxyphenyl)methylenedithiocarbazate; Salicylaldithiocarbazic acidmethyl ester

Suppliers and Price of methyl 2-[(Z)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of methyl 2-[(Z)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbodithioate

Chemical Property:

Vapor Pressure:2.56E-05mmHg at 25°C
Boiling Point:358.4°C at 760 mmHg
Flash Point:170.5°C
Density:1.415g/cm³

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 2-[(Z)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbodithioate

There total 2 articles about methyl 2-[(Z)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5397-03-5
hydrazinecarbodithioic acid methyl ester

: 90-02-8
salicylaldehyde

: 133978-98-0,26151-73-5
methyl 2-(2-hydroxybenzylidene)hydrazinecarbodithioate

Guidance literature:: In ethanol;
DOI:10.1039/DT9930001151

Reference yield:

: 133978-98-0,26151-73-5
methyl 2-(2-hydroxybenzylidene)hydrazinecarbodithioate

Guidance literature:

Reference yield: 95.0%

: ⁽⁹⁹⁾Tc(O)(CH₃SC(S)NNCHC₆H₄O)Cl

: 133978-98-0,26151-73-5
methyl 2-(2-hydroxybenzylidene)hydrazinecarbodithioate

: ⁽⁹⁹⁾Tc(N)(CH₃SC(S)NNCHC₆H₄O)(P(C₆H₅)3)

Guidance literature:: With triphenylphosphine; In ethanol; oxo complex, excess of ligand and PPh3 were mixed in refluxing ethanol for 15 min;; evapn. in vac., residue was washed with hot ethanol and Et2O, recrystd. from CH2Cl2 and ethanol; elem. anal.;;