2,6-DIMETHYLDECANE

Base Information

• Chemical Name: 2,6-DIMETHYLDECANE
• CAS No.: 13150-81-7
• Molecular Formula: C₁₂H₂₆
• Molecular Weight: 170.338
• Hs Code.: 2901100000
• Mol file: 13150-81-7.mol

Synonyms:2,6-Dimethyldecane

Chemical Property of 2,6-DIMETHYLDECANE

Chemical Property:

• Vapor Pressure: 0.454mmHg at 25°C
• Melting Point: -50.8°C (estimate)
• Refractive Index: 1.4187
• Boiling Point: 200.7°Cat760mmHg
• Flash Point: 130.6°C
• PSA: 0.00000
• Density: 0.749g/cm³
• LogP: 4.63900

Purity/Quality:

99%min ^*data from raw suppliers

2,6-Dimethyldecane ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi,F

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DIMETHYLDECANE

There total 5 articles about 2,6-DIMETHYLDECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dimethyl-2,6-decadiene (1674-06-2) → 2,6-dimethyldecane (13150-81-7)

Guidance literature:

With iron(II) bis(trimethylsilyl)amide; hydrogen; diisobutylaluminium hydride; at 20 ℃; under 1500.15 - 7500.75 Torr;

DOI:10.1039/c9ra07604b

Reference yield:

3,7-dimethylocta-2,6-dien-1-yl ethanoate (16409-44-2,8022-83-1) → 2,6-dimethyldecane (13150-81-7)

Guidance literature:

Multi-step reaction with 2 steps

1: iron(II) acetate; chloroform / diethyl ether / 1 h / 0 °C

2: hydrogen; diisobutylaluminium hydride; iron(II) bis(trimethylsilyl)amide / 20 °C / 1500.15 - 7500.75 Torr

With iron(II) bis(trimethylsilyl)amide; chloroform; hydrogen; iron(II) acetate; diisobutylaluminium hydride; In diethyl ether;

DOI:10.1039/c9ra07604b

Reference yield:

5,9-dimethyl-dec-8-en-5-ol (87386-18-3) → 2,6-dimethyldecane (13150-81-7)

Guidance literature:

With nickel pumice stone; hydrogen; at 200 - 205 ℃;

upstream raw materials:

5,9-dimethyl-dec-8-en-5-ol

3,7-dimethylocta-2,6-dien-1-yl ethanoate

2,6-dimethyl-2,6-decadiene

Refernces