11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine

Base Information

Chemical Name:11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine
CAS No.:69602-09-1
Molecular Formula:C₁₄H₁₇N₃
Molecular Weight:227.309
Hs Code.:
DSSTox Substance ID:DTXSID90989693

Synonyms:11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine;69602-09-1;10H-Quinuclidino(2,3-c)-1,5-benzodiazepine, 11,11a-dihydro-;DTXSID90989693;LS-143212;2,3,4,10,11,11a-Hexahydro-1,4-ethanopyrido[3,2-b][1,5]benzodiazepine

Suppliers and Price of 11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine

Chemical Property:

Vapor Pressure:4.23E-06mmHg at 25°C
Boiling Point:384°C at 760 mmHg
Flash Point:186°C
Density:1.38g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:227.142247555
Heavy Atom Count:17
Complexity:330

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN2CCC1C3=NC4=CC=CC=C4NCC32

Technology Process of 11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine

There total 3 articles about 11,11a-Dihydro-10H-quinuclidino(2,3-c)-1,5-benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5832-56-4
2-hydroxymethyl-3-hydroxy-Δ²-dehydroquinuclidine

: 95-54-5
1,2-diamino-benzene

: 69602-09-1
11,11a-dihydro-10H-benzodiazepino<3,4-b>quinuclidine

Guidance literature:: In ethanol; at 20 ℃; for 48h;
DOI:10.1007/BF00506040

Reference yield:

: 5291-26-9
2-methylenequinuclidin-3-one

: 69602-09-1
11,11a-dihydro-10H-benzodiazepino<3,4-b>quinuclidine

Guidance literature:: Multi-step reaction with 2 steps

1: 75.7 percent / H₂O / 48 h / 20 °C

2: 88 percent / ethanol / 48 h / 20 °C

With water; In ethanol;
DOI:10.1007/BF00506040