6H-Benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine, 5,8,13,13a-tetrahydro-10,11-dimethoxy-13-methyl-, cis-

Base Information

• Chemical Name: 6H-Benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine, 5,8,13,13a-tetrahydro-10,11-dimethoxy-13-methyl-, cis-
• CAS No.: 60734-46-5
• Molecular Formula: C21H23NO4
• Molecular Weight: 353.4116
• ChEMBL ID: CHEMBL3228979

Synonyms:CHEMBL3228979;NSC 276349;5,8,13,13a-Tetrahydro-10,11-dimethoxy-13-methyl-6H-benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine cis-;6H-Benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine, 5,8,13,13a-tetrahydro-10,11-dimethoxy-13-methyl-, cis-

Chemical Property of 6H-Benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine, 5,8,13,13a-tetrahydro-10,11-dimethoxy-13-methyl-, cis-

Chemical Property:

• Vapor Pressure: 6.75E-09mmHg at 25°C
• Boiling Point: 467°C at 760 mmHg
• Flash Point: 135°C
• Density: 1.3g/cm³
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 353.16270821
• Heavy Atom Count: 26
• Complexity: 516

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1C2C3=CC4=C(C=C3CCN2CC5=CC(=C(C=C15)OC)OC)OCO4
• Isomeric SMILES: C[C@@H]1[C@H]2C3=CC4=C(C=C3CCN2CC5=CC(=C(C=C15)OC)OC)OCO4

Technology Process of 6H-Benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine, 5,8,13,13a-tetrahydro-10,11-dimethoxy-13-methyl-, cis-

There total 2 articles about 6H-Benzo(g)-1,3-benzodioxolo(5,6-a)quinolizine, 5,8,13,13a-tetrahydro-10,11-dimethoxy-13-methyl-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 10,11-dimethoxy-13t-methyl-(13ar)-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline (60734-46-5,60734-47-6,79980-65-7,79980-68-0)

Guidance literature:

cis-Alkohol (10), 1. Methansulfonylchlorid/Pyridin, 2. NaCNBH3;

DOI:10.1021/jo00427a001

Reference yield:

→ 10,11-dimethoxy-13c-methyl-(13ar)-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline (60734-46-5,60734-47-6,79980-65-7,79980-68-0)

Guidance literature:

trans-Alkohol (9), 1. p-Tosylchlorid/Pyridin, 2. LiAlH4;

DOI:10.1021/jo00427a001

Reference yield:

10,11-dimethoxy-13c-methyl-(13ar)-5,8,13,13a-tetrahydro-6H-[1,3]dioxolo[4,5-g]isoquino[3,2-a]isoquinoline (60734-46-5,60734-47-6,79980-65-7,79980-68-0) → 2,3-methylenedioxy-10,11-dimethoxy-13-methylprotoberberine iodide (69776-36-9)

Guidance literature:

Multistep reaction; (i) Pd-C, AcOH, (ii) aq. NaI;

DOI:10.1021/jm00189a025

Downstream raw materials:

2,3-methylenedioxy-10,11-dimethoxy-13-methylprotoberberine iodide

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