2-Bromo-4-methyl-5-nitroanisole

Base Information

Chemical Name:2-Bromo-4-methyl-5-nitroanisole
CAS No.:41447-19-2
Molecular Formula:C8H8 Br N O3
Molecular Weight:246.06
Hs Code.:
NSC Number:140929
DSSTox Substance ID:DTXSID00301084
Wikidata:Q82044645

Synonyms:2-Bromo-4-methyl-5-nitroanisole;41447-19-2;1-bromo-2-methoxy-5-methyl-4-nitrobenzene;MFCD27935373;NSC140929;SCHEMBL8062327;3Bromo-4-methoxy-6-nitrotoluene;DTXSID00301084;JZBCPWGVPOVHAC-UHFFFAOYSA-N;AC1300;AKOS027256950;NSC-140929;CS-11635;SY027058;CS-0186582;A913447

Suppliers and Price of 2-Bromo-4-methyl-5-nitroanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of 2-Bromo-4-methyl-5-nitroanisole

Chemical Property:

Vapor Pressure:0.000854mmHg at 25°C
Boiling Point:314.6°Cat760mmHg
Flash Point:144°C
Density:1.559g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:244.96876
Heavy Atom Count:13
Complexity:194

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1[N+](=O)[O-])OC)Br

Technology Process of 2-Bromo-4-methyl-5-nitroanisole

There total 5 articles about 2-Bromo-4-methyl-5-nitroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 134-19-0
2-methoxy-4-nitro-5-methyl aniline

: 41447-19-2
1-bromo-2-methoxy-5-methyl-4-nitrobenzene

Guidance literature:: With hydrogen bromide; acetic acid; copper(I) bromide; sodium nitrite; In water;

Reference yield:

: 2042-14-0
4-methyl-5-nitrophenol

: 41447-19-2
1-bromo-2-methoxy-5-methyl-4-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform; bromine / 35 °C

2: K₂CO₃; xylene

With chloroform; bromine; potassium carbonate; xylene;
DOI:10.1039/jr9320002946

Reference yield:

: carbonic acid bis-(2-bromo-4-methyl-phenyl ester)

: 41447-19-2
1-bromo-2-methoxy-5-methyl-4-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: concentrated sulfuric acid; nitric acid / <10 / Erwaermen der Reaktionsprodukte mit wss. NaOH

2: K₂CO₃; xylene

With sulfuric acid; nitric acid; potassium carbonate; xylene;
DOI:10.1039/jr9320002946