Technology Process of 5-Hydroxytryptophol
There total 5 articles about 5-Hydroxytryptophol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5-Hydroxyindole-3-acetic acid;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
Inert atmosphere;
Reflux;
With
water;
In
tetrahydrofuran;
for 0.5h;
Cooling with ice;
- Guidance literature:
-
With
palladium on activated charcoal; ethanol;
Hydrogenation;
DOI:10.1021/jo01084a008
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaCN; aqueous ethanol
2: lithium alanate; diethyl ether
3: palladium/charcoal; ethanol / Hydrogenation
With
palladium on activated charcoal; lithium aluminium tetrahydride; diethyl ether; ethanol; sodium cyanide;
DOI:10.1021/jo01084a008