P-(1-Adamantyl)toluene

Base Information

• Chemical Name: P-(1-Adamantyl)toluene
• CAS No.: 1459-55-8
• Molecular Formula: C17H22
• Molecular Weight: 226.362
• Hs Code.: 2902909090
• Mol file: 1459-55-8.mol

Synonyms:Adamantane,1-p-tolyl- (7CI,8CI);1-(4-Methylphenyl)adamantane;1-(4-Tolyl)adamantane;1-(4'-Methylphenyl)adamantane;1-(p-Tolyl)adamantane;4-(1-Adamantyl)toluene;NSC 176093;Tricyclo[3.3.1.13,7]decane,1-(4-methylphenyl)-;

Chemical Property of P-(1-Adamantyl)toluene

Chemical Property:

• Melting Point: 99 °C
• Boiling Point: 329.5°Cat760mmHg
• Flash Point: 148.5°C
• PSA: 0.00000
• Density: 1.054 g/cm³
• LogP: 4.46280
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

p-(1-Adamantyl)toluene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: p-(1-Adamantyl)toluene exhibits sorption and sorbent properties and are used in chromatography.

Technology Process of P-(1-Adamantyl)toluene

There total 22 articles about P-(1-Adamantyl)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-adamanthanol (768-95-6) + toluene (108-88-3,15644-74-3,16713-13-6) → 4-(1-adamantyl)toluene (1459-55-8)

Guidance literature:

With indium(III) triflate; acetylacetone; for 2h; Reflux; Green chemistry;

DOI:10.1007/s11172-012-0239-7

Reference yield: 99.0%

1-Adamantyl bromide (768-90-1) + toluene (108-88-3,15644-74-3,16713-13-6) → 4-(1-adamantyl)toluene (1459-55-8)

Guidance literature:

With molybdenum hexacarbonyl; at 100 ℃; for 2h; Reagent/catalyst; Temperature; Time; regioselective reaction; Catalytic behavior; Sealed tube;

DOI:10.1134/S1070428015110056

Reference yield: 80.7%

1-Adamantyl bromide (768-90-1) + para-bromotoluene (106-38-7) → 4-(1-adamantyl)toluene (1459-55-8)

Guidance literature:

With magnesium; In diethyl ether; 1.) 0 deg C, 10 min; 2.) 100 deg C, 2 h;

DOI:10.1021/jo00292a027

upstream raw materials:

1-Adamantyl bromide

toluene

para-bromotoluene

1-chloroadamantane

Downstream raw materials:

1-(4-methyl-3-nitrophenyl)adamantane

2-(4-methylphenyl)adamantane

1-[4-(chloromethyl)phenyl]adamantane

1-chloro-3-p-tolyladamantane

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