6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt

Base Information

Chemical Name:6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt
CAS No.:102072-74-2
Molecular Formula:C₁₅H₇N₃O₇
Molecular Weight:341.236
Hs Code.:
Mol file:102072-74-2.mol

Synonyms:102072-74-2;6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt;5,8-Quinolinedione, 6-hydroxy-7-nitro-2-(2-nitrophenyl)-, sodium salt

Suppliers and Price of 6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt

Chemical Property:

Vapor Pressure:1.86E-13mmHg at 25°C
Boiling Point:561.8°C at 760 mmHg
Flash Point:293.5°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:1
Exact Mass:363.01034382
Heavy Atom Count:26
Complexity:663

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C2=NC3=C(C=C2)C(=O)C(=O)C(=C3[O-])[N+](=O)[O-])[N+](=O)[O-].[Na+]

Technology Process of 6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt

There total 3 articles about 6-Hydroxy-7-nitro-2-(2-nitrophenyl)-5,8-quinolinedione sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1466-88-2,66894-06-2
2-nitrocinnamic aldehyde

: 102072-74-2
2-(o-nitrophenyl)-6-hydroxy-7-nitro-5,8-quinolinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent / sodium m-nitrobenzenesulfonate / acetic acid / 1.5 h / 100 - 115 °C

2: 75 percent / NaClO₃, concd HCl / 2 h / 25 °C

3: NaNO₂ / acetone; H₂O / 0.25 h / Heating

With hydrogenchloride; sodium chlorate; sodium 3-nitrobenzenesulfonate; sodium nitrite; In water; acetic acid; acetone;
DOI:10.1021/jm00158a002

Reference yield:

: 61472-25-1
2-(o-nitrophenyl)-5,8-dimethoxyquinoline

: 102072-74-2
2-(o-nitrophenyl)-6-hydroxy-7-nitro-5,8-quinolinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaClO₃, concd HCl / 2 h / 25 °C

2: NaNO₂ / acetone; H₂O / 0.25 h / Heating

With hydrogenchloride; sodium chlorate; sodium nitrite; In water; acetone;
DOI:10.1021/jm00158a002

Reference yield:

: 102-56-7,102526-87-4
2,5-dimethoxyaniline

: 102072-74-2
2-(o-nitrophenyl)-6-hydroxy-7-nitro-5,8-quinolinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent / sodium m-nitrobenzenesulfonate / acetic acid / 1.5 h / 100 - 115 °C

2: 75 percent / NaClO₃, concd HCl / 2 h / 25 °C

3: NaNO₂ / acetone; H₂O / 0.25 h / Heating

With hydrogenchloride; sodium chlorate; sodium 3-nitrobenzenesulfonate; sodium nitrite; In water; acetic acid; acetone;
DOI:10.1021/jm00158a002