3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione

Base Information

Chemical Name:3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione
CAS No.:130598-05-9
Molecular Formula:C₁₅H₁₆O₆
Molecular Weight:292.288
Hs Code.:
DSSTox Substance ID:DTXSID40926816

Synonyms:BRN 4330350;3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione;2,4-Dioxaspiro(5,5)undecane-1,5,9-trione, 3,3-dimethyl-7-(2-furanyl)-;130598-05-9;DTXSID40926816;LS-62437;7-(FURAN-2-YL)-3,3-DIMETHYL-2,4-DIOXASPIRO[5.5]UNDECANE-1,5,9-TRIONE

Suppliers and Price of 3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione

Chemical Property:

Vapor Pressure:3.78E-12mmHg at 25°C
Boiling Point:550.1°C at 760 mmHg
Flash Point:286.5°C
Density:1.32g/cm³
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:1
Exact Mass:292.09468823
Heavy Atom Count:21
Complexity:474

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OC(=O)C2(CCC(=O)CC2C3=CC=CO3)C(=O)O1)C

Technology Process of 3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione

There total 2 articles about 3,3-Dimethyl-7-(2-furanyl)-2,4-dioxaspiro(5.5)undecane-1,5,9-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4755-95-7
5,5'-Methylen-bis(2,2-dimethyl-1,3-dioxan-4,6-dion)

: 73400-26-7
1-(2-furfuryl)-3-trimethylsilyloxy-1,3-butadiene

: 130598-05-9
2'-(2-furyl)-2,2-dimethyl-4,4',6-trioxo-1,3-dioxane-5-spiro-1'-cyclohexane

: 1'-methyl-3'-(2-furyl)-bis(2,2-dimethyl-4,6-dioxo-1,3-dioxane-5-spiro)-4',6'-(1'-cyclohexane)

Guidance literature:: With formaldehyd; prolina; In acetonitrile; for 1.5h; Ambient temperature;

Reference yield:

: 623-15-4
(E)-4-(furan-2-yl)but-3-en-2-one

: 130598-05-9
2'-(2-furyl)-2,2-dimethyl-4,4',6-trioxo-1,3-dioxane-5-spiro-1'-cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / zinc chloride, triethylamine / acetonitrile / 5 h / 50 °C

2: 0.7 g / 37percent aq. formalin, prolina / acetonitrile / 1.5 h

With formaldehyd; prolina; triethylamine; zinc(II) chloride; In acetonitrile;