(E)-N,N-Bis[4-(dimethylamino)butyl]-2-hexadecenamide

Base Information

• Chemical Name: (E)-N,N-Bis[4-(dimethylamino)butyl]-2-hexadecenamide
• CAS No.: 17232-86-9
• Molecular Formula: C28H57N3O
• Molecular Weight: 0
• Hs Code.: 2924199090
• Mol file: 17232-86-9.mol

Synonyms:SOLAPALMATININE;Solapalmitenine;Solapalmitenin;2-Hexadecenamide,N-bis[4-(dimethylamino)butyl]-,(E);

Chemical Property of (E)-N,N-Bis[4-(dimethylamino)butyl]-2-hexadecenamide

Chemical Property:

• Vapor Pressure: 1.2E-12mmHg at 25°C
• Boiling Point: 561.7°C at 760 mmHg
• Flash Point: 190°C
• PSA: 26.79000
• Density: 0.897g/cm³
• LogP: 6.75590

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: Solanum tripartitum Dunal yields two closely related alkaloids which have been found to possess marked antitumour activity. This base is a colourless oil, the structure of which has been established as trans-hexadec-2-enoylsolamine. Hydro_x0002_genation yields the dihydro derivative, identical with Solapalmitine (q.v.).

Technology Process of (E)-N,N-Bis[4-(dimethylamino)butyl]-2-hexadecenamide

There total 3 articles about (E)-N,N-Bis[4-(dimethylamino)butyl]-2-hexadecenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-dimethylaminobutyronitrile (13989-82-7) → Solapalmitenin (17232-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Rh-Al₂O₃

2: Me₃N

With hydrogen; trimethylamine; rhodium on alumina;

DOI:10.1021/jo01264a031

Reference yield:

solamine (17232-87-0) + (E)-Hexadec-14-enoyl chloride → Solapalmitenin (17232-86-9)

Guidance literature:

With trimethylamine;

DOI:10.1021/jo01264a031

Reference yield:

→ Solapalmitenin (17232-86-9)

Guidance literature:

Solanin, Hexadec-2t-enoylchlorid;

DOI:10.1021/ja00998a048

upstream raw materials:

solamine

4-dimethylaminobutyronitrile

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