3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate

Base Information

Chemical Name:3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
CAS No.:68808-54-8
Molecular Formula:C13H13N3•C2H4O2
Molecular Weight:271.35
Hs Code.:2933998090
European Community (EC) Number:815-098-8
DSSTox Substance ID:DTXSID0021416
Mol file:68808-54-8.mol

Synonyms:68808-54-8;Trp-P-1 acetate;3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate;Trp-P-1 (acetate);1,4-dimethyl-5H-pyrido[4,3-b]indol-3-amine acetate;CCRIS 1409;acetic acid;1,4-dimethyl-5H-pyrido[4,3-b]indol-3-amine;3-AMINO-1,4-DIMETHYL-5H-PYRIDO(4,3-B)INDOLE ACETATE;1,4-Dimethyl-5H-pyrido(4,3-b)indol-3-amine acetate;3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole,acetate;75104-43-7;5H-Pyrido(4,3-b)indol-3-amine, 1,4-dimethyl-, acetate;5H-Pyrido(4,3-b)indole, 3-amino-1,4-dimethyl-, acetate;5H-Pyrido(4,3-b)indol-3-amine, 1,4-dimethyl-, monoacetate;3-AMINO-1,4-DIMETHYL-5H-PYRIDO[4,3-B]INDOLE, ACETATE;3-Amino-1,4-dimethyl-5H-pyrido(4,3-b)indole monoacetate;3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole-13C2,15N Acetate;1217002-93-1;5H-Pyrido[4,3-b]indol-3-amine, 1,4-dimethyl-, monoacetate;3-AMINO-1,4-DIMETHYL-5H-PYRIDO[4,3-B]INDOLE MONOACETATE;SCHEMBL9185700;trp-p-1, acetate, AldrichCPR;DTXSID0021416;C13H13N3.C2H4O2;LS-7744;LS-133401;CS-0454904;FT-0614905;FT-0661771;1,4-dimethyl-5H-pyrido[4,3-b]indol-3-amineacetate;1,4-Dimethyl-5H-pyrido[4,3-b]indol-3-amine Monoacetate;3-AMINO-1,4-DIMETHYL-5-H-PYRIDO(4,3-B)INDOLE ACETATE

Suppliers and Price of 3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indoleAcetate
10mg
$ 175.00

SynQuest Laboratories
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
10 mg
$ 408.00

SynQuest Laboratories
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
5 mg
$ 336.00

SynQuest Laboratories
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
25 mg
$ 976.00

Medical Isotopes, Inc.
3-Amino-1,4-dimethyl-5h-pyrido[4,3-β]indoleAcetate
10 mg
$ 860.00

Biosynth Carbosynth
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
2 mg
$ 160.00

Biosynth Carbosynth
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
1 mg
$ 100.00

Biosynth Carbosynth
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
10 mg
$ 315.00

Biosynth Carbosynth
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
25 mg
$ 700.00

Biosynth Carbosynth
3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate
5 mg
$ 255.00

Total 11 raw suppliers

Chemical Property of 3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate

Chemical Property:

Vapor Pressure:1.19E-08mmHg at 25°C
Melting Point:250-260oC
Boiling Point:460.2°C at 760 mmHg
Flash Point:263°C
PSA：92.00000
LogP:3.58720
Storage Temp.:Refrigerator
Solubility.:DMSO (Slightly, Heated), Methanol (Slightly, Heated)
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:271.132076794
Heavy Atom Count:20
Complexity:299

Purity/Quality:

98%min ^*data from raw suppliers

3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indoleAcetate ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi,T
Hazard Codes:Xi,T
Statements: 25
Safety Statements: 45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=C(N=C1N)C)C3=CC=CC=C3N2.CC(=O)O

Technology Process of 3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate

There total 13 articles about 3-Amino-1,4-dimethyl-5H-pyrido[4,3-b]indole acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 128257-26-1
t-Boc-Trp-P-1

: 68808-54-8
Trp-P-1 acetate

Guidance literature:: With acetic acid; In water; at 80 ℃; for 1h;
DOI:10.1021/jo00048a026

Reference yield: 23.0%

: 76017-87-3
2-(1H-indol-2-yl)propionitrile

: 75-05-8,26809-02-9
acetonitrile

: 68808-54-8
Trp-P-1 acetate

Guidance literature:: aluminium trichloride; at 100 - 120 ℃; for 12h;
DOI:10.1248/cpb.29.1280

Reference yield:

: 52618-53-8
2-(cyanomethyl)-N-ethoxycarbonylindole

: 68808-54-8
Trp-P-1 acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / LDA / tetrahydrofuran / -78 deg C, 5 min, RT

2: 84 percent / potassium carbonate / methanol / 0.92 h / Ambient temperature

3: 23 percent / aluminum chloride / 12 h / 100 - 120 °C

With potassium carbonate; lithium diisopropyl amide; aluminium trichloride; In tetrahydrofuran; methanol;
DOI:10.1248/cpb.29.1280