1-tert-butyl-3,4-dimethyl-1H-phosphole

Base Information

Chemical Name:1-tert-butyl-3,4-dimethyl-1H-phosphole
CAS No.:38066-25-0
Molecular Formula:C₁₀H₁₇P
Molecular Weight:168.219
Hs Code.:

Synonyms:Tertiobutyl-1-dimethyl-3,4-phosphol;1-tert-Butyl-3,4-dimethyl-1H-phosphole;1-tert-butyl-3,4-dimethylphosphole;1-t-Butyl-3,4-dimethylphosphol;1-t-butyl-3,4-dimethylphosphole;

Suppliers and Price of 1-tert-butyl-3,4-dimethyl-1H-phosphole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tert-butyl-3,4-dimethyl-1H-phosphole

Chemical Property:

Boiling Point:35 - 36 °C (0.2 mmHg)
PSA：0.00000
LogP:4.04500

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-tert-butyl-3,4-dimethyl-1H-phosphole

There total 1 articles about 1-tert-butyl-3,4-dimethyl-1H-phosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 594-19-4
tert.-butyl lithium

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 38066-25-0
1-tert-butyl-3,4-dimethyl-phosphole

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; In hexane; pentane;
DOI:10.1016/S0040-4020(01)93648-8

Reference yield: 42.7%

: 64367-52-8
(1-phenyl-3,4-dimethylphosphole)heptacarbonyldiiron

: 38066-25-0
1-tert-butyl-3,4-dimethyl-phosphole

: 77611-25-7
μ-(1-phenyl-3,4-dimethylphosphole)-μ-(1-tert-butyl-3,4-dimethylphosphole)-bis(dicarbonyliron)

Guidance literature:: In xylene; soln. of compds. refluxed for 24 h, under Ar; cooled, filtered off, evapd., chromd. (hexane-benzene);
DOI:10.1021/ic50223a022

Reference yield:

: 38066-25-0
1-tert-butyl-3,4-dimethyl-phosphole

: 125657-25-2,149561-11-5
4-Phenyl-3a,6a-dihydro-3H-1,2-diaza-4-phospha-pentalene 4-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / H₂O

2: 20 percent / toluene / Irradiation

With water; In toluene;
DOI:10.1016/S0040-4039(00)99430-9