Tetrakis(4-(dimethylamino)phenyl)ethylene

Base Information

• Chemical Name: Tetrakis(4-(dimethylamino)phenyl)ethylene
• CAS No.: 86669-21-8
• Molecular Formula: C₃₄H₄₀N₄*2Cl
• Molecular Weight: 575.624
• Hs Code.: 2921590090
• DSSTox Substance ID: DTXSID701007004
• Mol file: 86669-21-8.mol

Synonyms:tetrakis(4-(dimethylamino)phenyl)ethylene;tetrakis(4-(dimethylamino)phenyl)ethylene dihydrochloride;TKDPE

Chemical Property of Tetrakis(4-(dimethylamino)phenyl)ethylene

Chemical Property:

• PSA: 12.50000
• LogP: -0.28780
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 574.2630027
• Heavy Atom Count: 40
• Complexity: 907

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)C(=C2C=CC(=[N+](C)C)C=C2)C(=C3C=CC(=[N+](C)C)C=C3)C4=CC=C(C=C4)N(C)C.[Cl-].[Cl-]

Technology Process of Tetrakis(4-(dimethylamino)phenyl)ethylene

There total 2 articles about Tetrakis(4-(dimethylamino)phenyl)ethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(p-dimethylaminophenyl)ethylene (1261-86-5) → tetrakisethylene dichloride (86669-21-8)

Guidance literature:

With tetrachloromethane; chlorine;

Reference yield:

bis(p-dimethylaminophenyl)methanone (90-94-8) → tetrakisethylene dichloride (86669-21-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 61 percent / Sn, conc. aq. HCl / 1.) RT, overnight, 2.) reflux, 2 h

2: 1.) phenyliodoso chloride, 2.) CCl₄ / 1.) CHCl₃, RT, 36 h , 2.) CHCl₃, RT, 48 h

With hydrogenchloride; tetrachloromethane; tin; phenyliodoso chloride;

DOI:10.1021/jm00365a018

Reference yield:

tetrakisethylene dichloride (86669-21-8) → tetrakis(p-dimethylaminophenyl)ethylene (1261-86-5)

Guidance literature:

beim Aufbewahren an feuchter Luft;

upstream raw materials:

tetrakis(p-dimethylaminophenyl)ethylene

bis(p-dimethylaminophenyl)methanone

Downstream raw materials:

tetrakis(p-dimethylaminophenyl)ethylene