1-hydroxy-2-[(E)-(3-methoxyphenyl)methylideneamino]guanidine;4-methylbenzenesulfonic acid

Base Information

Chemical Name:1-hydroxy-2-[(E)-(3-methoxyphenyl)methylideneamino]guanidine;4-methylbenzenesulfonic acid
CAS No.:87861-89-0
Molecular Formula:C₇H₈O₃S*C₉H₁₂N₄O₂
Molecular Weight:380.425
Hs Code.:
NSC Number:371165

Synonyms:87861-89-0;SCHEMBL2067088;NSC-371165

Suppliers and Price of 1-hydroxy-2-[(E)-(3-methoxyphenyl)methylideneamino]guanidine;4-methylbenzenesulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-hydroxy-2-[(E)-(3-methoxyphenyl)methylideneamino]guanidine;4-methylbenzenesulfonic acid

Chemical Property:

Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:380.11544092
Heavy Atom Count:26
Complexity:449

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)O.COC1=CC=CC(=C1)C=NN=C(N)NO
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)O.COC1=CC=CC(=C1)/C=N/N=C(/N)\NO

Technology Process of 1-hydroxy-2-[(E)-(3-methoxyphenyl)methylideneamino]guanidine;4-methylbenzenesulfonic acid

There total 3 articles about 1-hydroxy-2-[(E)-(3-methoxyphenyl)methylideneamino]guanidine;4-methylbenzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.1%

: 36826-58-1
N-hydroxy-N'-aminoguanidine p-toluenesulphonate

: 591-31-1
3-methoxy-benzaldehyde

: 87861-89-0
1-<(2-methoxybenzylidene)amino>-3-hydroxyguanidine tosylate

Guidance literature:: DOI:10.1021/jm00368a024

Reference yield:

: 36778-68-4
S-methylisothiosemicarbazide tosylate

: 87861-89-0
1-<(2-methoxybenzylidene)amino>-3-hydroxyguanidine tosylate

Guidance literature:: Multi-step reaction with 2 steps

1: 44.2 percent / hydroxylamine / 48 h / Ambient temperature

2: 69.1 percent

With hydroxylamine;
DOI:10.1021/jm00368a024

Reference yield:

: 80-48-8
methyl p-toluene sulfonate

: 87861-89-0
1-<(2-methoxybenzylidene)amino>-3-hydroxyguanidine tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: 135 g / CH₃OH / 18 h / Heating

2: 44.2 percent / hydroxylamine / 48 h / Ambient temperature

3: 69.1 percent

With methanol; hydroxylamine;
DOI:10.1021/jm00368a024