2-Allylthio-2-ethylbutyramide

Base Information

• Chemical Name: 2-Allylthio-2-ethylbutyramide
• CAS No.: 64037-65-6
• Molecular Formula: C₉H₁₇NOS
• Molecular Weight: 187.306
• Hs Code.: 2930909090
• Mol file: 64037-65-6.mol

Synonyms:Butanamide,2-ethyl-2-(2-propenylthio)- (9CI); Butyramide, 2-(allylthio)-2-ethyl-(6CI,7CI); NSC 37883

Chemical Property of 2-Allylthio-2-ethylbutyramide

Chemical Property:

• Vapor Pressure: 0.000751mmHg at 25°C
• Refractive Index: 1.5250 (estimate)
• Boiling Point: 306.9°C at 760 mmHg
• Flash Point: 139.4°C
• PSA: 68.39000
• Density: 1.001g/cm³
• LogP: 2.65000

Purity/Quality:

99% ^*data from raw suppliers

2-ALLYLTHIO-2-ETHYLBUTYRAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Allylthio-2-ethylbutyramide

There total 3 articles about 2-Allylthio-2-ethylbutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethyl-2-allylmercapto-butyryl chloride (90722-39-7) → 2-Allylmercapto-2-ethyl-buttersaeure-amid (64037-65-6)

Guidance literature:

With ammonia; water;

Reference yield:

2-mercapto-2-ethylbutyric acid (52988-77-9) → 2-Allylmercapto-2-ethyl-buttersaeure-amid (64037-65-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium ethylate; ethanol / anschliessendes Behandeln mit Allylbromid

2: thionyl chloride

3: water; ammonia

With thionyl chloride; ethanol; ammonia; water; sodium ethanolate;

Reference yield:

2-ethyl-2-allylmercapto-butyric acid (90646-84-7) → 2-Allylmercapto-2-ethyl-buttersaeure-amid (64037-65-6)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: water; ammonia

With thionyl chloride; ammonia; water;

upstream raw materials:

2-ethyl-2-allylmercapto-butyryl chloride

2-mercapto-2-ethylbutyric acid

2-ethyl-2-allylmercapto-butyric acid