3,4-Dinitrophenyl-N-acetylglucosaminide

Base Information

Chemical Name:3,4-Dinitrophenyl-N-acetylglucosaminide
CAS No.:71693-36-2
Molecular Formula:C14H17N3O10
Molecular Weight:387.303
Hs Code.:
DSSTox Substance ID:DTXSID80221918
Wikidata:Q83099966
Mol file:71693-36-2.mol

Synonyms:3,4-dinitrophenyl-N-acetyl-beta-D-glucosaminide;3,4-dinitrophenyl-N-acetylglucosaminide;3,4-DPNAG

Suppliers and Price of 3,4-Dinitrophenyl-N-acetylglucosaminide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3,4-DINITROPHENYL-N-ACETYL-BETA-D-GLUCOSAMINIDE 95.00%
5MG
$ 497.90

Total 2 raw suppliers

Chemical Property of 3,4-Dinitrophenyl-N-acetylglucosaminide

Chemical Property:

PSA：203.38000
LogP:0.71220
Storage Temp.:?20°C
XLogP3:-0.7
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:4
Exact Mass:387.09139375
Heavy Atom Count:27
Complexity:564

Purity/Quality:: 3,4-DINITROPHENYL-N-ACETYL-BETA-D-GLUCOSAMINIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1C(C(C(OC1OC2=CC(=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])CO)O)O
Isomeric SMILES:CC(=O)N[C@@H]1[C@H]([C@@H]([C@H](O[C@H]1OC2=CC(=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])CO)O)O

Technology Process of 3,4-Dinitrophenyl-N-acetylglucosaminide

There total 3 articles about 3,4-Dinitrophenyl-N-acetylglucosaminide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,4-dinitrophenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 71693-36-2
3,4-dinitrophenyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 1h;
DOI:10.1021/ja0567687

Reference yield:

: 66-56-8
2,3-dinitrophenol

: 71693-36-2
3,4-dinitrophenyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: benzyltriethylammonium chloride; aq. NaOH / CH₂Cl₂ / 20 °C

2: sodium methoxide / methanol / 1 h / 20 °C

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/ja0567687

Reference yield:

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 71693-36-2
3,4-dinitrophenyl 2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: benzyltriethylammonium chloride; aq. NaOH / CH₂Cl₂ / 20 °C

2: sodium methoxide / methanol / 1 h / 20 °C

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/ja0567687