1,5-Di-p-toluidinoanthraquinone

Base Information

• Chemical Name: 1,5-Di-p-toluidinoanthraquinone
• CAS No.: 82-20-2
• Deprecated CAS: 59459-28-8,67577-84-8,72146-56-6
• Molecular Formula: C28H22N2O2
• Molecular Weight: 418.495
• European Community (EC) Number: 232-338-1,201-403-6,614-081-0
• NSC Number: 13985
• DSSTox Substance ID: DTXSID30864132
• Nikkaji Number: J192.599G
• Wikidata: Q82854495
• Mol file: 82-20-2.mol

Synonyms:1,5-Di-p-toluidinoanthraquinone;8005-40-1;82-20-2;Violet 3R base;1,5-bis(4-methylanilino)anthracene-9,10-dione;n-Hydroxy succinate;Morplas Violet 14;SOLVENT VIOLET 14;EINECS 201-403-6;EINECS 232-338-1;NSC 13985;C.I. 61705;1,5-Bis(p-tolylamino)anthracene-9,10-dione;9,10-Anthracenedione, 1,5-bis((4-methylphenyl)amino)-;9,10-Anthracenedione, 1,5-bis[(4-methylphenyl)amino]-;9,10-Anthracenedione, 1,5(or 1,8)-bis((4-methylphenyl)amino)-;9,10-Anthracenedione, 1,5(or 1,8)-bis[(4-methylphenyl)amino]-;1,5(Or1,8)-bis((4-methylphenyl)amino)anthraquinone;1,5(or1,8)-bis[(4-methylphenyl)amino]anthraquinone;NSC13985;Dyes, Solvent Violet 14;1,5-Bis[(4-methylphenyl)amino]-9,10-anthracenedione;SCHEMBL7152111;Anthraquinone,5-di-p-toluidino-;DTXSID30864132;1,5-Di-(p-Toluidino)-anthrachinon;Anthraquinone, 1,5-di-p-toluidino-;NSC-13985;9, 1,5-bis[(4-methylphenyl)amino]-;1,5-bis(4-methylphenyl)amino]anthraquinon;1,5-bis(4-methylphenyl)amino]anthraquinone;1,5-Bis((4-methylphenyl)amino)anthraquinone;FT-0607032;1,5-Bis(4-methylphenylamino)anthracene-9,10-dione;67577-84-8

Chemical Property of 1,5-Di-p-toluidinoanthraquinone

Chemical Property:

• XLogP3: 7.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 418.168127949
• Heavy Atom Count: 32
• Complexity: 619

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)NC2=CC=CC3=C2C(=O)C4=C(C3=O)C(=CC=C4)NC5=CC=C(C=C5)C

Technology Process of 1,5-Di-p-toluidinoanthraquinone

There total 7 articles about 1,5-Di-p-toluidinoanthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

1,5-Dichloroanthraquinone (82-46-2) + p-toluidine (106-49-0,12221-03-3) → 1,5-bis(4-methylphenyl)aminoanthraquinone (82-20-2) + 1-chloro-5-(4-methylphenyl)aminoanthraquinone (3098-20-2)

Guidance literature:

for 0.25h; Heating;

DOI:10.1021/jo01298a044

Reference yield:

1,5-Dichloroanthraquinone (82-46-2) + p-toluidine (106-49-0,12221-03-3) → 1,5-bis(4-methylphenyl)aminoanthraquinone (82-20-2)

Guidance literature:

Reference yield:

1.5-dinitroanthraquinone (82-35-9) + p-toluidine (106-49-0,12221-03-3) → 1,5-bis(4-methylphenyl)aminoanthraquinone (82-20-2) + 1-nitro-5-p-toluidino-anthraquinone (49852-99-5)

Guidance literature:

With pyridine;

upstream raw materials:

1,5-Dichloroanthraquinone

p-toluidine

1.5-dinitroanthraquinone

1,5-anthraquinone disulfonate

Downstream raw materials:

NSC 297168