2-benzoyl-3-chloro-1H-phenalen-1-one

Base Information

Chemical Name:2-benzoyl-3-chloro-1H-phenalen-1-one
CAS No.:214597-35-0
Molecular Formula:C20H11ClO2
Molecular Weight:318.759
Hs Code.:
DSSTox Substance ID:DTXSID30382922
Wikidata:Q82174399
Mol file:214597-35-0.mol

Synonyms:2-benzoyl-3-chlorophenalen-1-one;2-benzoyl-3-chloro-1H-phenalen-1-one;214597-35-0;DTXSID30382922;CCG-236053

Suppliers and Price of 2-benzoyl-3-chloro-1H-phenalen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-benzoyl-3-chloro-1H-phenalen-1-one

Chemical Property:

Vapor Pressure:7.58E-10mmHg at 25°C
Boiling Point:492.6°C at 760 mmHg
Flash Point:206.5°C
Density:1.39g/cm³
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:318.0447573
Heavy Atom Count:23
Complexity:544

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C2=C(C3=CC=CC4=C3C(=CC=C4)C2=O)Cl

Technology Process of 2-benzoyl-3-chloro-1H-phenalen-1-one

There total 3 articles about 2-benzoyl-3-chloro-1H-phenalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 214597-34-9
2-Benzoyl-3-hydroxyphenalen-1H-one

: 214597-35-0
2-benzoyl-1-chloro-3-phenalenone

Guidance literature:: With triethylamine; trichlorophosphate; for 1h; Heating;
DOI:10.1002/jhet.5570350427

Reference yield:

: 5472-84-4
3-hydroxy-phenalen-1-one

: 214597-35-0
2-benzoyl-1-chloro-3-phenalenone

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / Et₃N / toluene / 12 h / Heating

2: 16 percent / AlCl₃ / CH₂Cl₂ / 12 h / Ambient temperature

3: 94 percent / POCl₃, NEt₃ / 1 h / Heating

With aluminium trichloride; triethylamine; trichlorophosphate; In dichloromethane; toluene;
DOI:10.1002/jhet.5570350427

Reference yield:

: 22517-19-7
3-benzoyloxyphenalen-1-one

: 214597-35-0
2-benzoyl-1-chloro-3-phenalenone

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / AlCl₃ / CH₂Cl₂ / 12 h / Ambient temperature

2: 94 percent / POCl₃, NEt₃ / 1 h / Heating

With aluminium trichloride; triethylamine; trichlorophosphate; In dichloromethane;
DOI:10.1002/jhet.5570350427