1-Hydroxydibenzothiophene

Base Information

Chemical Name:1-Hydroxydibenzothiophene
CAS No.:69747-83-7
Molecular Formula:C12H8OS
Molecular Weight:200.261
Hs Code.:
DSSTox Substance ID:DTXSID40220043
Nikkaji Number:J1.697.709H
Wikidata:Q83097111

Synonyms:1-Hydroxydibenzothiophene;69747-83-7;dibenzothiophen-1-ol;Dibenzothiophene-1-ol;CCRIS 5305;hydroxydibenzothiophene;Dibenzo[b,d]thiophen-1-ol;SCHEMBL2338956;DTXSID40220043;WMULKBIXKMJJBM-UHFFFAOYSA-N;FT-0741982

Suppliers and Price of 1-Hydroxydibenzothiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Hydroxydibenzothiophene

Chemical Property:

Vapor Pressure:4.37E-07mmHg at 25°C
Boiling Point:403.4°C at 760 mmHg
Flash Point:197.8°C
Density:1.375g/cm³
XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:200.02958605
Heavy Atom Count:14
Complexity:218

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=C(C=CC=C3S2)O

Technology Process of 1-Hydroxydibenzothiophene

There total 1 articles about 1-Hydroxydibenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1013-23-6
Dibenzothiophene sulfoxide

: 132-64-9,214827-48-2
dibenzofuran

: 132-65-0
dibenzothiophene

: 69747-83-7
1-Hydroxydibenzothiophene

Guidance literature:: at 700 ℃; under 0.001 - 0.01 Torr; Product distribution; flash vacuum pyrolysis, other temperature;
DOI:10.1021/jo00181a019

Reference yield: 28.0%

: 69747-83-7
1-Hydroxydibenzothiophene

: 1210-39-5
3,3-diphenyl-2-propenal

: 2,2-diphenyl-[2H]-pyran[6,5-a]dibenzothiophene

Guidance literature:: With titanium(IV) tetraethanolate; In toluene; for 3h; Heating;
DOI:10.1016/S0040-4020(02)00023-6

Reference yield:

: 69747-83-7
1-Hydroxydibenzothiophene

: C₃₆H₂₅N₃OS

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / Reflux

2: sulfuric acid; acetic acid

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Reflux

4: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 2 h / Reflux; Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium acetate; potassium carbonate; caesium carbonate; acetic acid; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; 4: |Suzuki Coupling;