4-Methyl-2,6-bis(1-phenylethyl)phenol

Base Information

• Chemical Name: 4-Methyl-2,6-bis(1-phenylethyl)phenol
• CAS No.: 1817-68-1
• Molecular Formula: C23H24 O
• Molecular Weight: 316.443
• Hs Code.: 2907199090
• European Community (EC) Number: 217-328-7
• DSSTox Substance ID: DTXSID0051813
• Nikkaji Number: J120.232D
• Mol file: 1817-68-1.mol

Synonyms:4-Methyl-2,6-bis(1-phenylethyl)phenol;Ionol 6;Alkofen MBP;1817-68-1;2,6-Bis(1-phenylethyl)-p-cresol;EINECS 217-328-7;UNII-65T4T73YKT;2,6-Bis(1-phenylethyl)-4-methylphenol;Phenol, 4-methyl-2,6-bis(1-phenylethyl)-;2,6-Bis(alpha-methylbenzyl)-p-cresol;2,6-Bis(.alpha.-methylbenzyl)-p-cresol;p-CRESOL, 2,6-BIS(alpha-METHYLBENZYL)-;SCHEMBL224197;65T4T73YKT;DTXSID0051813;C23H24O;2,6-bis(methylbenzyl)-4-methylphenol;LS-55325;2,6-DI(ALPHA-METHYL BENZYL)-4-METHYL PHENOL

Chemical Property of 4-Methyl-2,6-bis(1-phenylethyl)phenol

Chemical Property:

• Vapor Pressure: 3.05E-08mmHg at 25°C
• Refractive Index: 1.6380 (estimate)
• Boiling Point: 436.9°Cat760mmHg
• Flash Point: 203.9°C
• PSA: 20.23000
• Density: 1.063g/cm³
• LogP: 6.00420
• XLogP3: 6.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 316.182715385
• Heavy Atom Count: 24
• Complexity: 332

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,6-BIS(1-PHENYLETHYL)-P-CRESOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C(C)C2=CC=CC=C2)O)C(C)C3=CC=CC=C3

Technology Process of 4-Methyl-2,6-bis(1-phenylethyl)phenol

There total 5 articles about 4-Methyl-2,6-bis(1-phenylethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.6%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + p-cresol (106-44-5) → 4-methyl-2-(1-phenylethyl)phenol (1817-67-0,53520-20-0) + meso-2,6-di(α-methylbenzyl)-4-methylphenol (1817-68-1)

Guidance literature:

With Fe-Al-MCM-41; In cyclohexane; at 85 ℃; for 4h; Temperature; Time; Catalytic behavior;

DOI:10.33224/rrch.2020.65.2.03

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + p-cresol (106-44-5) → meso-2,6-di(α-methylbenzyl)-4-methylphenol (1817-68-1)

Guidance literature:

With aluminium;

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + p-cresol (106-44-5) → 4-methyl-2-(1-phenylethyl)phenol (1817-67-0,53520-20-0) + meso-2,6-di(α-methylbenzyl)-4-methylphenol (1817-68-1) + 2,5-di(α-methylbenzyl)-4-methylphenol (108959-38-2) + 2,6-di(α-methylbenzyl)-4-methylphenol (1817-68-1,108959-36-0,108959-37-1)

Guidance literature:

With aluminium tris(p-methylphenoxide); at 130 ℃; for 2h; Product distribution; var. conc., var. temp., var. time;

upstream raw materials:

styrene

p-cresol

Refernces

• 1、 An, Lianying,Feng, Zhenhua,Huang, Zhenggen,Wang, Bengao,Zhao, Xianyin. "Catalytic synthesis of 4-methyl-2-(α-methyl benzyl) phenol over fe-al-mcm-41 for extraction-separation rubidium from brine". . p. 141 - 147. Retrieved 2020/10/06.