Nsc40742

Base Information

• Chemical Name: Nsc40742
• CAS No.: 6973-62-2
• Molecular Formula: C10H16O5
• Molecular Weight: 216.234
• Mol file: 6973-62-2.mol

Synonyms:NSC 40742;

Chemical Property of Nsc40742

Chemical Property:

• Vapor Pressure: 0.00202mmHg at 25°C
• Refractive Index: 1.441
• Boiling Point: 290.9 °C at 760 mmHg
• Flash Point: 124.5 °C
• Density: 1.109 g/cm³

Purity/Quality:

99% ^*data from raw suppliers

2,5-BishydroxymethylTetrahydrofuranDiacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nsc40742

There total 5 articles about Nsc40742 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrahydrofuran-2,5-dimethanol (104-80-3,1122-89-0,2144-40-3,81370-88-9,81370-89-0) + acetic anhydride (108-24-7) → 2,5-Bis-acetoxymethyl-tetrahydro-furan (6973-62-2)

Guidance literature:

With sodium acetate;

Reference yield:

1,5-Hexadien (592-42-7) → 2,5-Bis-acetoxymethyl-tetrahydro-furan (6973-62-2)

Guidance literature:

With peracetic acid;

Reference yield:

1,5-hexadiene diepoxide (1888-89-7,74892-51-6,74892-53-8,131722-62-8) → 2,5-Bis-acetoxymethyl-tetrahydro-furan (6973-62-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water / 16 h / 20 °C

2: pyridine / 2 h / 0 °C

With pyridine; sodium hydroxide; In water;

DOI:10.2174/1570178612666150819194241

upstream raw materials:

tetrahydrofuran-2,5-dimethanol

acetic anhydride

1,5-Hexadien

1,6-diiodo-hexane-2,5-diol

Downstream raw materials:

1,2,5,6-hexanetetrol