10-Bromodecanoic acid

Base Information

• Chemical Name: 10-Bromodecanoic acid
• CAS No.: 50530-12-6
• Molecular Formula: C10H19BrO2
• Molecular Weight: 251.164
• Hs Code.: 29159000
• Mol file: 50530-12-6.mol

Synonyms:Capricacid, i-bromo- (4CI);10-Bromodecanoicacid;

Chemical Property of 10-Bromodecanoic acid

Chemical Property:

• Appearance/Colour: White to light green Solid
• Vapor Pressure: 1.72E-05mmHg at 25°C
• Melting Point: 38-41 °C(lit.)
• Refractive Index: 1.484
• Boiling Point: 339.2 °C at 760 mmHg
• PKA: 4.78±0.10(Predicted)
• Flash Point: 158.9 °C
• PSA: 37.30000
• Density: 1.247 g/cm³
• LogP: 3.58670
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature
• Water Solubility.: Partly miscible in water.

Purity/Quality:

99% ^*data from raw suppliers

10-Bromodecanoic Acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 10-Bromodecanoic acid may be employed as an alkylcarboxylate chain source in the preparation of alkylcarboxylate-grafted polyethylenimine. It may also be used in the synthesis of :10-(methylsulfinyl)decanoic acid10-cyanodecanoic acid(10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)-decyl)triphenylphosphonium bromide11-thiastearic acid

Technology Process of 10-Bromodecanoic acid

There total 14 articles about 10-Bromodecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-bromo-10-(tetrahydropyranyloxy)decane (51795-88-1) → 10-bromodecanoic acid (50530-12-6)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In acetone;

DOI:10.1016/S0968-0896(97)00072-2

Reference yield: 92.0%

1-undecen-11-ylbromide (7766-50-9) → 10-bromodecanoic acid (50530-12-6)

Guidance literature:

With potassium permanganate; tetrabutylammomium bromide; In water; benzene; for 6h; Ambient temperature;

DOI:10.1021/jo00017a027

Reference yield: 75.0%

10-hydroxydecanoic acid (1679-53-4) → 10-bromodecanoic acid (50530-12-6)

Guidance literature:

With hydrogen bromide; acetic acid; a) r.t., 16 h, b) 100 deg C, 4 h;

upstream raw materials:

10-hydroxydecanoic acid

1-bromo-10-decanol

1-undecen-11-ylbromide

10-bromodecanal

Downstream raw materials:

ethyl 10-bromo-decanoate

10-bromodecanoic acid methyl ester

methyl undecanoate

methyl cis-13-docosenoate

Refernces

• 1、 -. "RENEWABLY DERIVED POLYAMIDES AND METHODS OF MAKING THE SAME". Paragraph 0084. . Retrieved 2018/05/23.
• 2、 Nakamura,Setodoi,Hanasaki. "Syntheses and physical properties of ferrocene derivatives (XIII)". . p. 93 - 101. Retrieved 2007/10/03.