5-IODO-6-METHYLURACIL

Base Information

• Chemical Name: 5-IODO-6-METHYLURACIL
• CAS No.: 1461-67-2
• Molecular Formula: C5H5IN2O2
• Molecular Weight: 252.011
• Hs Code.: 2933599090
• Mol file: 1461-67-2.mol

Synonyms:Uracil,5-iodo-6-methyl- (6CI,7CI,8CI);5-Iodo-6-methyluracil;NSC 266138;

Chemical Property of 5-IODO-6-METHYLURACIL

Chemical Property:

• Melting Point: 280 °C (dec.)(lit.)
• Refractive Index: 1.666
• PKA: 8.07±0.10(Predicted)
• PSA: 65.72000
• Density: 2.17 g/cm³
• LogP: -0.02380
• Storage Temp.: -20°C

Purity/Quality:

99% ^*data from raw suppliers

5-Iodo-6-methylpyrimidine-2,4-diol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 40-42/43
• Safety Statements: 22-26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-IODO-6-METHYLURACIL

There total 4 articles about 5-IODO-6-METHYLURACIL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

6-Methyluracil (626-48-2) → 5-iodine-6-methyl-1H-pyrimidine-2,4-dione (1461-67-2)

Guidance literature:

With dihydrogen peroxide; acetic acid; potassium iodide; at 20 - 25 ℃; Reagent/catalyst; Solvent; Concentration; Time;

DOI:10.1007/s10593-012-1094-z

Reference yield: 95.0%

2,4-dihydroxy-6-methylpyrimidine (626-48-2) → 5-Iod-6-methyl-uracil (1461-67-2)

Guidance literature:

With N-iodo-succinimide; acetic acid; for 7h;

Reference yield:

→ 5-Iod-6-methyl-uracil (1461-67-2)

Guidance literature:

4-Methyluracil, I2, wss. KOH;

upstream raw materials:

6-Methyluracil

2,4-dihydroxy-6-methylpyrimidine

Downstream raw materials:

1,2,3,4-Tetrahydro-5-iodo-1,3,6-trimethyl-2,4-dioxopyrimidine

C₂₃H₂₅IN₂O₅

1,3-dibenzyl-5-iodo-6-phenethyluracil

5-bromo-6-methyluracil

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