N-(1-cyclohexylethylideneamino)-2,4-dinitroaniline

Base Information

• Chemical Name: N-(1-cyclohexylethylideneamino)-2,4-dinitroaniline
• CAS No.: 1160-74-3
• Molecular Formula: C14H18N4O4
• Molecular Weight: 306.321
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID30921895
• Mol file: 1160-74-3.mol

Synonyms:1160-74-3;1-(1-cyclohexylethylidene)-2-(2,4-dinitrophenyl)hydrazine;N-(1-cyclohexylethylideneamino)-2,4-dinitroaniline;DTXSID30921895;AKOS034405379

Chemical Property of N-(1-cyclohexylethylideneamino)-2,4-dinitroaniline

Chemical Property:

• Vapor Pressure: 2.99E-08mmHg at 25°C
• Boiling Point: 448.9°Cat760mmHg
• Flash Point: 225.3°C
• PSA: 116.03000
• Density: 1.39g/cm³
• LogP: 4.99050
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 306.13280507
• Heavy Atom Count: 22
• Complexity: 437

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])C2CCCCC2

Technology Process of N-(1-cyclohexylethylideneamino)-2,4-dinitroaniline

There total 7 articles about N-(1-cyclohexylethylideneamino)-2,4-dinitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cyclohexyl methyl ketone (823-76-7) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → Cyclohexyl methyl ketone 2,4-dinitrophenylhydrazone (1160-74-3)

Guidance literature:

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) → Cyclohexyl methyl ketone 2,4-dinitrophenylhydrazone (1160-74-3)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted alcohol

With ethanol;

Reference yield:

cyclohexanecarbaldehyde (2043-61-0) → Cyclohexyl methyl ketone 2,4-dinitrophenylhydrazone (1160-74-3)

Guidance literature:

Multi-step reaction with 2 steps

2: 10percent aq. HCl / methanol / 1 h / Ambient temperature

With hydrogenchloride; In methanol;

DOI:10.1055/s-1988-27522

upstream raw materials:

Cyclohexyl methyl ketone

(2,4-dinitro-phenyl)-hydrazine

1-(2-Methoxyaethoxy)-aethylidencyclohexan

cyclohexanecarbaldehyde

Downstream raw materials:

Cyclohexyl methyl ketone

benzene-1,2,4-triamine