Technology Process of [(1E)-cycloocten-1-yl] 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
There total 3 articles about [(1E)-cycloocten-1-yl] 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
dichloromethane;
cooled down solution of (n-C4F9SO2)2O to -15°C, then stirring for 2 days at room temp.;
- Guidance literature:
-
In
1,2-dimethoxyethane;
the Na salt of the ketone is prepared in the react. mixture from NaH and the corresponding ketone, at 0°C C4F9SO2F is added, stirring 1 h, refluxed at 50-60°C, 15 h;
- Guidance literature:
-
With
sodium carbonate;
In
dichloromethane;
