2-Iodo-2-propenal

Base Information

Chemical Name:2-Iodo-2-propenal
CAS No.:99414-73-0
Molecular Formula:C3H3 I O
Molecular Weight:181.961
Hs Code.:2913000090
DSSTox Substance ID:DTXSID20244060
Nikkaji Number:J3.278.002D
Wikidata:Q83128338
Mol file:99414-73-0.mol

Synonyms:2-Iodo-2-propenal;2-Propenal, 2-iodo-;99414-73-0;SCHEMBL2526360;DTXSID20244060

Suppliers and Price of 2-Iodo-2-propenal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Iodo-2-propenal

Chemical Property:

Vapor Pressure:1.06mmHg at 25°C
Boiling Point:177.1°Cat760mmHg
Flash Point:60.9°C
PSA：17.07000
Density:2.042g/cm³
LogP:1.13400
XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:181.92286
Heavy Atom Count:5
Complexity:57.9

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C=O)I

Technology Process of 2-Iodo-2-propenal

There total 2 articles about 2-Iodo-2-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 107-02-8,25068-14-8
acrolein

: 99414-73-0
α-iodo acrolein

Guidance literature:: With iodine; triethylamine; In diethyl ether; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/ejoc.201101430

Reference yield:

: 107-02-8,25068-14-8
acrolein

: 99414-73-0
α-iodo acrolein

Guidance literature:

Reference yield: 91.0%

: 99414-73-0
α-iodo acrolein

: 6926-44-9
phenethyl azide

: 1-(2-phenylethyl)-1H-1,2,3-triazole-4-carbaldehyde

Guidance literature:: α-iodo acrolein; phenethyl azide; In water; dimethyl sulfoxide; at 20 ℃; for 36h;

With triethylamine; In water; dimethyl sulfoxide; at 20 ℃; for 0.0833333h; regioselective reaction;
DOI:10.1039/c9gc01129c