13,28-Epoxyolean-11-ene-3β,16β-diol

Base Information

• Chemical Name: 13,28-Epoxyolean-11-ene-3β,16β-diol
• CAS No.: 13715-23-6
• Molecular Formula: C30H48O3
• Molecular Weight: 456.70032
• Mol file: 13715-23-6.mol

Synonyms:

Chemical Property of 13,28-Epoxyolean-11-ene-3β,16β-diol

Chemical Property:

• PSA: 49.69000
• LogP: 6.12850

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 13,28-Epoxyolean-11-ene-3β,16β-diol

There total 5 articles about 13,28-Epoxyolean-11-ene-3β,16β-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.4%

saikosaponin c → saikogenin E (13715-23-6,79786-12-2) + prosapogenin E3 + prosapogenin E2 + prosapogenin E1

Guidance literature:

With sodium; In ethanol; for 36h; Ambient temperature;

DOI:10.1039/c39860001417

Reference yield:

saikogenin E 3-O-β-D-glucopyranosyl-(1→6)-[α-L-rhamnopyranosyl-(1→4)]-β-D-glucopyranoside → saikogenin E (13715-23-6)

Guidance literature:

With mouse intestinal flora; In ethanol; at 37 ℃; for 12h;

DOI:10.1248/cpb.33.3349

Reference yield:

saikosaponin c → prosaikosaponin E-3 (106452-35-1) + prosaikogenin E-2 + prosaikogenin E-1 + saikogenin E (13715-23-6,79786-12-2)

Guidance literature:

With sodium; In butan-1-ol; at 80 ℃; for 6h;

upstream raw materials:

Corchorusin D

Refernces

• 1、 Nose, Mitsuhiko,Amagaya, Sakae,Takeda, Tadahiro,Ogihara, Yukio. "New Derivatives of Saikosaponin c". . p. 1293 - 1296. Retrieved 2007/10/02.
• 2、 Ogihara, Yukio,Nose, Mitsuhiko. "Novel Cleavage of the Glycosidic Bond of Saponins in Alcoholic Alkali Metal Solution containing a Trace of Water". . p. 1417. Retrieved 2007/10/02.