2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one

Base Information

Chemical Name:2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one
CAS No.:67065-98-9
Molecular Formula:C14H9ClO5
Molecular Weight:292.6713
Hs Code.:
NSC Number:294887
DSSTox Substance ID:DTXSID90418554
Wikidata:Q75063403
Metabolomics Workbench ID:117735

Synonyms:67065-98-9;NSC294887;7-Chlornorlichexanthone;7-Chloro-norlichexanthone;DTXSID90418554;CHEBI:144176;AKOS005266851;NSC-294887;2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one

Suppliers and Price of 2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one

Chemical Property:

Vapor Pressure:4.72E-14mmHg at 25°C
Boiling Point:580°C at 760 mmHg
Flash Point:304.6°C
Density:1.652g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:0
Exact Mass:292.0138511
Heavy Atom Count:20
Complexity:403

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=CC2=C1C(=O)C3=C(C=C(C=C3O2)O)O)O)Cl

Technology Process of 2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one

There total 7 articles about 2-Chloro-3,6,8-trihydroxy-1-methyl-9H-xanthen-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 131524-53-3
6-benzyloxy-7-chloro-1,3-dihydroxy-8-methyl-9H-xanthen-9-one

: 67065-98-9
7-chloro-1,3,6-trihydroxy-8-methyl-9H-xanthen-9-one

Guidance literature:: With boron trichloride; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1071/CH9901745

Reference yield: 76.0%

: 131524-54-4
7-chloro-1,3,6-trihydroxy-8-methyl-9-oxo-9H-xanthen-2-carboxylic acid

: 67065-98-9
7-chloro-1,3,6-trihydroxy-8-methyl-9H-xanthen-9-one

Guidance literature:: With potassium hydroxide; In water; dimethyl sulfoxide; at 100 - 110 ℃; for 5h;
DOI:10.1071/CH9901745

Reference yield:

: 131524-51-1
benzyl 6-benzyloxy-7-chloro-1,3-dihydroxy-8-methyl-9-oxo-9H-xanthen-2-carboxylate

: 67065-98-9
7-chloro-1,3,6-trihydroxy-8-methyl-9H-xanthen-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / KOH / dimethylsulfoxide; H₂O / 5 h / 100 - 110 °C

2: 81 percent / boron trichloride / CH₂Cl₂ / 2 h / Ambient temperature

With potassium hydroxide; boron trichloride; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1071/CH9901745