3-O-Fucopyranosyl-2-acetamido-2-deoxyglucopyranose

Base Information

Chemical Name:3-O-Fucopyranosyl-2-acetamido-2-deoxyglucopyranose
CAS No.:52630-68-9
Molecular Formula:C₁₄H₂₅NO₁₀
Molecular Weight:367.353
Hs Code.:
DSSTox Substance ID:DTXSID00967068
Wikidata:Q82949569
Metabolomics Workbench ID:39002
Mol file:52630-68-9.mol

Synonyms:3-O-fucopyranosyl-2-acetamido-2-deoxyglucopyranose;Fuc-1-3-GlcNAc

Suppliers and Price of 3-O-Fucopyranosyl-2-acetamido-2-deoxyglucopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Acetamido-2-deoxy-3-O-(α-L-fucopyranosyl)-D-glucopyranose
5mg
$ 155.00

TRC
2-Acetamido-2-deoxy-3-O-(α-L-fucopyranosyl)-D-glucopyranose
2mg
$ 120.00

Chem-Impex
Fucα(1-3)GlcNAc
5MG
$ 666.27

Total 8 raw suppliers

Chemical Property of 3-O-Fucopyranosyl-2-acetamido-2-deoxyglucopyranose

Chemical Property:

Melting Point:>155°C (dec.)
Boiling Point:792.9°Cat760mmHg
Flash Point:433.3°C
PSA：186.01000
Density:1.49g/cm³
LogP:-3.99230
Storage Temp.:-20°C Freezer
XLogP3:-4.5
Hydrogen Bond Donor Count:7
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:8
Exact Mass:367.14784599
Heavy Atom Count:25
Complexity:449

Purity/Quality:

99% ^*data from raw suppliers

2-Acetamido-2-deoxy-3-O-(α-L-fucopyranosyl)-D-glucopyranose ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(C(C(C(O1)OC(C(C=O)NC(=O)C)C(C(CO)O)O)O)O)O
Isomeric SMILES:C[C@H]1[C@H]([C@H]([C@@H]([C@@H](O1)O[C@H]([C@H](C=O)NC(=O)C)[C@@H]([C@@H](CO)O)O)O)O)O

Technology Process of 3-O-Fucopyranosyl-2-acetamido-2-deoxyglucopyranose

There total 4 articles about 3-O-Fucopyranosyl-2-acetamido-2-deoxyglucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 50711-25-6
benzyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-α-D-glucopyranoside

: 52630-68-9
2-acetamido-2-deoxy-3-O-(α-L-fucopyranosyl)-D-glucose

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; water; at 50 ℃; for 48h;
DOI:10.1007/s11172-015-0990-7

Reference yield:

: 116514-50-2,128962-63-0,131545-02-3,136758-06-0,99409-34-4,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 52630-68-9
2-acetamido-2-deoxy-3-O-(α-L-fucopyranosyl)-D-glucose

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammomium bromide; copper(ll) bromide / dichloromethane; N,N-dimethyl-formamide / 4 h / 21 °C / Molecular sieve

1.2: 64 h / 21 °C / Molecular sieve

2.1: trifluoroacetic acid / chloroform; water / 0.5 h / 27 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol; water / 48 h / 50 °C

With palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; trifluoroacetic acid; copper(ll) bromide; In ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1007/s11172-015-0990-7

Reference yield:

: 78246-81-8
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 52630-68-9
2-acetamido-2-deoxy-3-O-(α-L-fucopyranosyl)-D-glucose

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammomium bromide; copper(ll) bromide / dichloromethane; N,N-dimethyl-formamide / 4 h / 21 °C / Molecular sieve

1.2: 64 h / 21 °C / Molecular sieve

2.1: trifluoroacetic acid / chloroform; water / 0.5 h / 27 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol; water / 48 h / 50 °C

With palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; trifluoroacetic acid; copper(ll) bromide; In ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1007/s11172-015-0990-7