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1-Oxaspiro[4.5]dec-3-ene

Base Information Edit
  • Chemical Name:1-Oxaspiro[4.5]dec-3-ene
  • CAS No.:1004-57-5
  • Molecular Formula:C9H14O
  • Molecular Weight:
  • Hs Code.:
  • Mol file:1004-57-5.mol
1-Oxaspiro[4.5]dec-3-ene

Synonyms:

Suppliers and Price of 1-Oxaspiro[4.5]dec-3-ene
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 2 raw suppliers
Chemical Property of 1-Oxaspiro[4.5]dec-3-ene Edit
Chemical Property:
Purity/Quality:

95% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of 1-Oxaspiro[4.5]dec-3-ene

There total 1 articles about 1-Oxaspiro[4.5]dec-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
gold(III) chloride; In acetonitrile; Further Variations:; catalyst amount; Product distribution;
DOI:10.1002/ejoc.200600009
Guidance literature:
Multi-step reaction with 3 steps
1: 54 percent / MCPBA / CH2Cl2 / 20 °C
2: 95 percent / LDA / tetrahydrofuran / 20 °C
3: 78 percent / NaH (60 percent in mineral oil) / tetrahydrofuran / 0.5 h / 65 °C
With sodium hydride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 1: Epoxidation / 2: Rearrangement / 3: Etherification;
DOI:10.1002/1099-0690(200009)2000:18<3145::AID-EJOC3145>3.0.CO;2-B
upstream raw materials:

1-propa-1,2-dienylcyclohexan-1-ol

Refernces Edit
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